2-Diazo-1,1,3,3-tetramethylcyclohexane

Base Information

• Chemical Name: 2-Diazo-1,1,3,3-tetramethylcyclohexane
• CAS No.: 89050-90-8
• Molecular Formula: C10H18N2
• Molecular Weight: 166.266
• DSSTox Substance ID: DTXSID80528318
• Nikkaji Number: J699.355I
• Wikidata: Q82397825

Synonyms:89050-90-8;2-Diazo-1,1,3,3-tetramethylcyclohexane;DTXSID80528318;2,2,6,6-tetramethyldiazocyclohexane

Chemical Property of 2-Diazo-1,1,3,3-tetramethylcyclohexane

Chemical Property:

• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 166.146998583
• Heavy Atom Count: 12
• Complexity: 214

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1(CCCC(C1=[N+]=[N-])(C)C)C

Technology Process of 2-Diazo-1,1,3,3-tetramethylcyclohexane

There total 2 articles about 2-Diazo-1,1,3,3-tetramethylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,2,6,6-Tetramethylcyclohexanon-p-tolylsulfonylhydrazon (89050-81-7) → 2-diazo-1,1',3,3'-tetramethylcyclohexane (89050-90-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; 1) reflux, 4 h, 2) 130 deg C, 3 h, 0.1 Torr;

Reference yield: 83.0%

2,2,6,6-tetramethylcyclohexanone hydrazone (87842-38-4) → 2-diazo-1,1',3,3'-tetramethylcyclohexane (89050-90-8)

Guidance literature:

With barium manganate; calcium oxide; In tetrachloromethane; for 2h;

DOI:10.1016/S0040-4020(01)96723-7

Reference yield: 100.0%

2,2-dimethylpropylidynephosphine (78129-68-7) + 2-diazo-1,1',3,3'-tetramethylcyclohexane (89050-90-8) → 3-tert-Butyl-6,6,10,10-tetramethyl-1,2-diaza-4-phospha-spiro[4.5]deca-1,3-diene (111557-84-7)

Guidance literature:

In pentane; at -40 ℃;

upstream raw materials:

2,2,6,6-tetramethylcyclohexanone hydrazone

2,2,6,6-Tetramethylcyclohexanon-p-tolylsulfonylhydrazon

Downstream raw materials:

3-tert-Butyl-6,6,10,10-tetramethyl-1,2-diaza-4-phospha-spiro[4.5]deca-1,3-diene

2,4,6-tri(tert-butyl)benzaldehyde

3'-(2,4,6-tri-t-butylphenyl)-2,2,6,6-tetramethylspiro

2,2,6,6-tetramethyl-1-cyclohexane

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