Cyclohexene, 4,5-bis(iodomethyl)-, cis-

Base Information

Chemical Name:Cyclohexene, 4,5-bis(iodomethyl)-, cis-
CAS No.:89088-83-5
Molecular Formula:C8H12I2
Molecular Weight:361.992
Hs Code.:

Synonyms:4r,5c-bis-iodomethyl-cyclohexene;(4S,5R)-4,5-Bis-iodomethyl-cyclohexene;cis-4.5-Bis-(jodmethyl)-cyclohexen;4r,5c-Bis-jodmethyl-cyclohexen;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexene, 4,5-bis(iodomethyl)-, cis-

Chemical Property:

PSA：0.00000
LogP:3.43880

Purity/Quality:

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Technology Process of Cyclohexene, 4,5-bis(iodomethyl)-, cis-

There total 6 articles about Cyclohexene, 4,5-bis(iodomethyl)-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 439919-46-7
cis-1,6-dihydroxymethyl-3-cyclohexene

: 89088-83-5
rel-(4R,5S)-4,5-bis(iodomethyl)cyclohex-1-ene

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/ol401823m

Reference yield: 70.0%

: 25886-60-6,439919-48-9
((1R,6S)-6-{[(methylsulfonyl)oxy]methyl}cyclohex-3-en-1-yl)methyl methanesulfonate

: 89088-83-5
rel-(4R,5S)-4,5-bis(iodomethyl)cyclohex-1-ene

Guidance literature:: With sodium iodide; In acetone; Reflux;
DOI:10.1016/j.bmcl.2009.11.118

Reference yield:

: 935-79-5
cis-1,2,3,6-tetrahydrophthalic anhydride

: 89088-83-5
rel-(4R,5S)-4,5-bis(iodomethyl)cyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran

2: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 3 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; iodine; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/ol401823m