4-Methyl-N-(4-methylphenyl)-N-[4-(2-phenylethenyl)phenyl]aniline

Base Information

Chemical Name:4-Methyl-N-(4-methylphenyl)-N-[4-(2-phenylethenyl)phenyl]aniline
CAS No.:89114-75-0
Molecular Formula:C₂₈H₂₅N
Molecular Weight:375.513
Hs Code.:
DSSTox Substance ID:DTXSID80694885
Mol file:89114-75-0.mol

Synonyms:89114-75-0;DTXSID80694885;FT-0734623;4-Methyl-N-(4-methylphenyl)-N-[4-(2-phenylethenyl)phenyl]aniline

Suppliers and Price of 4-Methyl-N-(4-methylphenyl)-N-[4-(2-phenylethenyl)phenyl]aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 4-Methyl-N-(4-methylphenyl)-N-[4-(2-phenylethenyl)phenyl]aniline

Chemical Property:

Melting Point:172-173 °C
Boiling Point:556.2±50.0 °C(Predicted)
PKA:-2.51±0.50(Predicted)
PSA：3.24000
Density:1.116
LogP:7.94360
XLogP3:8.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:375.198699802
Heavy Atom Count:29
Complexity:458

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N(C2=CC=C(C=C2)C)C3=CC=C(C=C3)C=CC4=CC=CC=C4

Technology Process of 4-Methyl-N-(4-methylphenyl)-N-[4-(2-phenylethenyl)phenyl]aniline

There total 9 articles about 4-Methyl-N-(4-methylphenyl)-N-[4-(2-phenylethenyl)phenyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 108-86-1,52753-63-6
bromobenzene

: 106-38-7
para-bromotoluene

: 1520-21-4,25086-42-4
4-vinyl benzylamine

: 89114-75-0
N,N-bis(4-methylphenyl)-4-[2-phenylethenyl]benzenamine

Guidance literature:: para-bromotoluene; 4-vinyl benzylamine; With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,8,9-tris(2-methylpropyl)-2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane; In toluene; at 85 ℃; for 3h;

bromobenzene; In toluene; at 110 ℃; for 16h; Product distribution / selectivity;

Reference yield: 90.0%

: 42906-19-4
4-[N,N-di(p-tolyl)amino]benzaldehyde

: 1449-46-3
benzyltriphenylphosphonium bromide

: 89114-75-0
4-(4,4'-dimethyldiphenylamino)stilbene

Guidance literature:: benzyltriphenylphosphonium bromide; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

4-[N,N-di(p-tolyl)amino]benzaldehyde; In tetrahydrofuran; at 80 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c4tc00860j

Reference yield: 81.0%

: 591-50-4
iodobenzene

: 624-31-7
4-tolyl iodide

: 1520-21-4,25086-42-4
4-vinyl benzylamine

: 89114-75-0
N,N-bis(4-methylphenyl)-4-[2-phenylethenyl]benzenamine

Guidance literature:: 4-tolyl iodide; 4-vinyl benzylamine; With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,8,9-tris(2-methylpropyl)-2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane; In toluene; at 60 ℃; for 3h;

iodobenzene; In toluene; at 110 ℃; for 16h; Product distribution / selectivity;