Technology Process of 2-Hexanone, 6-chloro-3-[(phenylthio)methylene]-
There total 3 articles about 2-Hexanone, 6-chloro-3-[(phenylthio)methylene]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / Et3N / CHCl3 / 2 h / 20 °C
2: 1.) N-chlorosuccinimide; 2.) Et3N / 1.) CCl4, 0 deg C, 2 h; 2.) CHCl3, reflux, 1.5 h, then 20 deg C, 12 h
With
N-chloro-succinimide; triethylamine;
In
chloroform;
DOI:10.1016/S0040-4020(01)88610-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 59 percent / p-toluenesulfonic acid / benzene / 2 h / Heating
2: 98 percent / Et3N / CHCl3 / 2 h / 20 °C
3: 1.) N-chlorosuccinimide; 2.) Et3N / 1.) CCl4, 0 deg C, 2 h; 2.) CHCl3, reflux, 1.5 h, then 20 deg C, 12 h
With
N-chloro-succinimide; toluene-4-sulfonic acid; triethylamine;
In
chloroform; benzene;
DOI:10.1016/S0040-4020(01)88610-5
- Guidance literature:
-
With
N-chloro-succinimide; triethylamine;
Yield given. Multistep reaction;
1.) CCl4, 0 deg C, 2 h; 2.) CHCl3, reflux, 1.5 h, then 20 deg C, 12 h;
DOI:10.1016/S0040-4020(01)88610-5
