1-Methoxy-1,5-bis(phenylsulfanyl)pentan-2-one

Base Information

Chemical Name:1-Methoxy-1,5-bis(phenylsulfanyl)pentan-2-one
CAS No.:89171-39-1
Molecular Formula:C₁₈H₂₀O₂S₂
Molecular Weight:332.488
Hs Code.:
DSSTox Substance ID:DTXSID60519709

Synonyms:89171-39-1;1-METHOXY-1,5-BIS(PHENYLSULFANYL)PENTAN-2-ONE;DTXSID60519709

Suppliers and Price of 1-Methoxy-1,5-bis(phenylsulfanyl)pentan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methoxy-1,5-bis(phenylsulfanyl)pentan-2-one

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:332.09047222
Heavy Atom Count:22
Complexity:310

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(C(=O)CCCSC1=CC=CC=C1)SC2=CC=CC=C2

Technology Process of 1-Methoxy-1,5-bis(phenylsulfanyl)pentan-2-one

There total 1 articles about 1-Methoxy-1,5-bis(phenylsulfanyl)pentan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13865-50-4
methoxymethyl phenyl sulfide

: 89171-34-6
N,N-Dimethyl-4-phenylsulfanyl-butyramide

: 89171-39-1
1-Methoxy-1,5-bis-phenylsulfanyl-pentan-2-one

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h; 2.) -78 deg C, 1 h;
DOI:10.1246/cl.1983.1909

Reference yield: 72.0%

: 1067-74-9
Methyl diethylphosphonoacetate

: 89171-39-1
1-Methoxy-1,5-bis-phenylsulfanyl-pentan-2-one

: 89171-48-2,89171-49-3
(Z)-3-(Methoxy-phenylsulfanyl-methyl)-6-phenylsulfanyl-hex-2-enoic acid methyl ester

Guidance literature:: In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1246/cl.1983.1909

Reference yield:

: 89171-39-1
1-Methoxy-1,5-bis-phenylsulfanyl-pentan-2-one

: 89171-61-9
3-(3-Phenylsulfanyl-propyl)-furan

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / tetrahydrofuran / 12 h / Ambient temperature

2: 92 percent / DIBAL / diethyl ether / 1.5 h / -30 °C

3: 86 percent / p-toluenesulfonic acid / benzene / 1 h / Heating

With diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1246/cl.1983.1909