6-Chloro-2-methyl-4-phenyl-3,4-dihydroquinoline;hydrobromide

Base Information

Chemical Name:6-Chloro-2-methyl-4-phenyl-3,4-dihydroquinoline;hydrobromide
CAS No.:89228-24-0
Molecular Formula:C16H14ClN.BrH
Molecular Weight:336.659
Hs Code.:
DSSTox Substance ID:DTXSID10519855

Synonyms:89228-24-0;DTXSID10519855;6-Chloro-2-methyl-4-phenyl-3,4-dihydroquinoline--hydrogen bromide (1/1)

Suppliers and Price of 6-Chloro-2-methyl-4-phenyl-3,4-dihydroquinoline;hydrobromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Chloro-2-methyl-4-phenyl-3,4-dihydroquinoline;hydrobromide

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:335.00764
Heavy Atom Count:19
Complexity:319

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC2=C(C=C(C=C2)Cl)C(C1)C3=CC=CC=C3.Br

Technology Process of 6-Chloro-2-methyl-4-phenyl-3,4-dihydroquinoline;hydrobromide

There total 5 articles about 6-Chloro-2-methyl-4-phenyl-3,4-dihydroquinoline;hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 89228-10-4
4-<5-chloro-2-(N-benzyloxycarbonylamino)>-phenyl-4-phenylbutan-2-one

: 89228-24-0
2-methyl-4-phenyl-6-chloro-3,4-dihydroquinoline hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 0.166667h; Ambient temperature;
DOI:10.1016/S0040-4020(01)91589-3

Reference yield:

: 1896-62-4
(E)-benzalacetone

: 89228-24-0
2-methyl-4-phenyl-6-chloro-3,4-dihydroquinoline hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / TBA(+)Cl(-) / PdCl₂ / CH₂Cl₂; aq. HCl / 5 h / Ambient temperature

2: 95 percent / 37percent HBr / acetic acid / 0.17 h / Ambient temperature

With tetrabutyl-ammonium chloride; hydrogen bromide; palladium dichloride; In hydrogenchloride; dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(01)91589-3

Reference yield:

: 2-(N-benzyloxycarbonylamino)-5-chlorophenylmercury chloride

: 89228-24-0
2-methyl-4-phenyl-6-chloro-3,4-dihydroquinoline hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / TBA(+)Cl(-) / PdCl₂ / CH₂Cl₂; aq. HCl / 5 h / Ambient temperature

2: 95 percent / 37percent HBr / acetic acid / 0.17 h / Ambient temperature

With tetrabutyl-ammonium chloride; hydrogen bromide; palladium dichloride; In hydrogenchloride; dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(01)91589-3