Technology Process of Phenol, 2,6-dimethyl-4-[(2,4,6-trimethylphenyl)amino]-
There total 8 articles about Phenol, 2,6-dimethyl-4-[(2,4,6-trimethylphenyl)amino]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1: 85 percent / formic acid (90percent), acetic anhydride / 3 h / Heating
2: NaOH, zinc dust / H2O; ethanol / 1 h / Heating
3: 78 percent / ammonium acetate, potassium ferricyanide / H2O; tetrahydrofuran / 240 h / 45 °C
4: 75 percent / ascorbic acid / H2O; methanol
With
ammonium acetate; sodium hydroxide; formic acid; acetic anhydride; ascorbic acid; potassium hexacyanoferrate(III); zinc;
In
tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/jo00183a024
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / ceric ammonium nitrate / acetic acid / 0.5 h / Heating
2: 85 percent / formic acid (90percent), acetic anhydride / 3 h / Heating
3: NaOH, zinc dust / H2O; ethanol / 1 h / Heating
4: 78 percent / ammonium acetate, potassium ferricyanide / H2O; tetrahydrofuran / 240 h / 45 °C
5: 75 percent / ascorbic acid / H2O; methanol
With
ammonium acetate; sodium hydroxide; formic acid; ammonium cerium(IV) nitrate; acetic anhydride; ascorbic acid; potassium hexacyanoferrate(III); zinc;
In
tetrahydrofuran; methanol; ethanol; water; acetic acid;
DOI:10.1021/jo00183a024