2-Cyclopropylidenecyclohexan-1-one

Base Information

Chemical Name:2-Cyclopropylidenecyclohexan-1-one
CAS No.:89237-72-9
Molecular Formula:C9H12O
Molecular Weight:136.194
Hs Code.:
DSSTox Substance ID:DTXSID50508006
Wikidata:Q82364668

Synonyms:89237-72-9;2-Cyclopropylidenecyclohexanone;2-Cyclopropylidenecyclohexan-1-one;DTXSID50508006

Suppliers and Price of 2-Cyclopropylidenecyclohexan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclopropylidenecyclohexan-1-one

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:136.088815002
Heavy Atom Count:10
Complexity:195

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(=O)C(=C2CC2)C1

Technology Process of 2-Cyclopropylidenecyclohexan-1-one

There total 2 articles about 2-Cyclopropylidenecyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 66115-38-6
cyclopropylidene-2 dimethoxy-1,1 cyclohexane

: 89237-72-9
cyclopropylidene-2 cyclohexanone

Guidance literature:: With water; silica gel; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(01)91580-7

Reference yield:

: 38461-13-1
2,2-dimethoxycyclohexanone

: 89237-72-9
cyclopropylidene-2 cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) DME, r.t. 2) DME, 80 deg C, 36 h

2: 60 percent / SiO₂, H₂O / CH₂Cl₂ / 3 h / Ambient temperature

With water; silica gel; sodium hydride; In dichloromethane;
DOI:10.1016/S0040-4020(01)91580-7

Reference yield: 74.0%

: 89237-72-9
cyclopropylidene-2 cyclohexanone

: 89238-02-8
cyclopropylidene-2 cyclohexanol-1

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; at 0 ℃; for 0.0833333h;
DOI:10.1016/S0040-4020(01)91581-9