1-Chloro-4-[1,2,2-tris(4-chlorophenyl)ethenyl]benzene

Base Information

• Chemical Name: 1-Chloro-4-[1,2,2-tris(4-chlorophenyl)ethenyl]benzene
• CAS No.: 78525-36-7
• Molecular Formula: C26H16 Cl4
• Molecular Weight: 470.225
• NSC Number: 403645
• DSSTox Substance ID: DTXSID70323354
• Nikkaji Number: J408.523J
• Wikidata: Q82082318

Synonyms:78525-36-7;Tetrakis(4-chlorophenyl)ethene;1,1,2,2-Tetrakis(4-chlorophenyl)ethene;1-chloro-4-[1,2,2-tris(4-chlorophenyl)ethenyl]benzene;NSC403645;C26H16Cl4;tetrakis(p-chlorophenyl)ethylene;DTXSID70323354;NSC 403645;NSC-403645;CS-0379222;1-chloro-4-[1,2,2-tris(4-chlorophenyl)vinyl]benzene

Chemical Property of 1-Chloro-4-[1,2,2-tris(4-chlorophenyl)ethenyl]benzene

Chemical Property:

• Boiling Point: 526.8°Cat760mmHg
• Flash Point: 261.7°C
• Density: 1.33g/cm³
• XLogP3: 10.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 4
• Exact Mass: 469.997661
• Heavy Atom Count: 30
• Complexity: 458

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=C(C2=CC=C(C=C2)Cl)C3=CC=C(C=C3)Cl)C4=CC=C(C=C4)Cl)Cl

Technology Process of 1-Chloro-4-[1,2,2-tris(4-chlorophenyl)ethenyl]benzene

There total 17 articles about 1-Chloro-4-[1,2,2-tris(4-chlorophenyl)ethenyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + bromochlorobenzene (106-39-8) → 1,1,2,2-tetrakis(4-chlorophenyl)ethene (78525-36-7)

Guidance literature:

With iron(III) chloride hexahydrate; sodium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; at 100 ℃; for 24h;

DOI:10.3906/kim-1701-31

Reference yield: 83.0%

4,4'-dichlorobenzophenone hydrazone (5463-11-6) → 1,1,2,2-tetrakis(4-chlorophenyl)ethene (78525-36-7)

Guidance literature:

With triethylamine; diselenium dibromide; In benzene; for 2h; Heating;

DOI:10.1002/ejoc.200300510

Reference yield: 65.0%

4,4'-dichlorothiobenzophenone (3705-95-1) → 1,1,2,2-tetrakis(4-chlorophenyl)ethene (78525-36-7)

Guidance literature:

With copper; In dimethyl sulfoxide; for 15h; Ambient temperature;

upstream raw materials:

1-[bromo(4-chlorophenyl)methyl]-4-chlorobenzene

triisopropyl phosphite

4,4'-Dichlorobenzophenone

4,4'-dichlorothiobenzophenone

Downstream raw materials:

1,2-dichloro-1,1,2,2-tetrakis-(4-chloro-phenyl)-ethane

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