3,3'-(2,2-Dichloroethene-1,1-diyl)bis(6-methoxyaniline)

Base Information

Chemical Name:3,3'-(2,2-Dichloroethene-1,1-diyl)bis(6-methoxyaniline)
CAS No.:89264-25-5
Molecular Formula:C16H16Cl2N2O2
Molecular Weight:339.221
Hs Code.:
DSSTox Substance ID:DTXSID70522264
Wikidata:Q82387387

Synonyms:89264-25-5;3,3'-(2,2-Dichloroethene-1,1-diyl)bis(6-methoxyaniline);DTXSID70522264

Suppliers and Price of 3,3'-(2,2-Dichloroethene-1,1-diyl)bis(6-methoxyaniline)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-(2,2-Dichloroethene-1,1-diyl)bis(6-methoxyaniline)

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:338.0588831
Heavy Atom Count:22
Complexity:372

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(=C(Cl)Cl)C2=CC(=C(C=C2)OC)N)N

Technology Process of 3,3'-(2,2-Dichloroethene-1,1-diyl)bis(6-methoxyaniline)

There total 4 articles about 3,3'-(2,2-Dichloroethene-1,1-diyl)bis(6-methoxyaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.1%

: 89264-23-3
1,1-dichloro-2,2-bis(4-methoxy-3-nitrophenyl)ethylene

: 89264-25-5
1,1-dichloro-2,2-bis(4-methoxy-3-aminophenyl)ethylene

Guidance literature:: With hydrogenchloride; tin(ll) chloride; In methanol; for 1h; Heating;

Reference yield:

: 91-23-6
2-Nitroanisole

: 89264-25-5
1,1-dichloro-2,2-bis(4-methoxy-3-aminophenyl)ethylene

Guidance literature:: Multi-step reaction with 3 steps

1: fuming sulfuric acid; concentrated sulfuric acid / 65 - 70 °C

2: ethanol; benzene; ethanolic KOH

3: Raney nickel; ethanol / Hydrogenation

With potassium hydroxide; ethanol; sulfuric acid; nickel; benzene;
DOI:10.1021/ja01177a066

Reference yield:

: 72-43-5,105367-23-5
Methoxychlor

: 89264-25-5
1,1-dichloro-2,2-bis(4-methoxy-3-aminophenyl)ethylene

Guidance literature:: Multi-step reaction with 3 steps

1: glacial acetic acid; concentrated nitric acid

2: ethanol; benzene; ethanolic KOH

3: Raney nickel; ethanol / Hydrogenation

With potassium hydroxide; ethanol; nitric acid; nickel; acetic acid; benzene;
DOI:10.1021/ja01177a066