1-methyl-4-phenyl-2,3-dihydropyridinium perchlorate

Base Information

• Chemical Name: 1-methyl-4-phenyl-2,3-dihydropyridinium perchlorate
• CAS No.: 97467-07-7
• Molecular Formula: C12H14ClNO4
• Molecular Weight: 271.6969

Synonyms:1-Methyl-4-phenyl-2,3-dihydropyridinium perchlorate;1-methyl-4-phenyl-5,6-dihydropyridine perchlorate;

Chemical Property of 1-methyl-4-phenyl-2,3-dihydropyridinium perchlorate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 77.28000
• Density: g/cm³
• LogP: 2.35990

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-methyl-4-phenyl-2,3-dihydropyridinium perchlorate

There total 1 articles about 1-methyl-4-phenyl-2,3-dihydropyridinium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2-cyano-1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine (97187-62-7) → 1-methyl-4-phenyl-2,3-dihydropyridine perchlorate (97467-07-7)

Guidance literature:

With perchloric acid; at 5 ℃; for 120h;

DOI:10.1021/jm00148a010

Reference yield: 76.0%

potassium cyanide (151-50-8) + 1-methyl-4-phenyl-2,3-dihydropyridine perchlorate (97467-07-7) → 2-cyano-1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine (97187-62-7)

Guidance literature:

With phosphate buffer; at 37 ℃; for 12h;

DOI:10.1021/jm00148a010

Reference yield: 8.0%

1-methyl-4-phenyl-2,3-dihydropyridine perchlorate (97467-07-7) → 2-methyl-5-methylene-4a,6-diphenyl-2,3,4,4a,5,8-hexahydroisoquinoline (118459-64-6)

Guidance literature:

With potassium phosphate buffer pH 7.4; In water; at 37 ℃; for 2h;

DOI:10.1021/jo00266a011

upstream raw materials:

2-cyano-1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine

Downstream raw materials:

1,2,5,6-tetrahydro-1-methyl-4-phenyl-2-pyridine carbonitrile

2-cyano-1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine

2-methyl-5-methylene-4a,6-diphenyl-2,3,4,4a,5,8-hexahydroisoquinoline

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