[1-(Benzyloxy)but-3-en-2-yl](trimethyl)stannane

Base Information

• Chemical Name: [1-(Benzyloxy)but-3-en-2-yl](trimethyl)stannane
• CAS No.: 89358-34-9
• Molecular Formula: C₁₄H₂₂OSn
• Molecular Weight: 325.038
• DSSTox Substance ID: DTXSID70526742

Synonyms:89358-34-9;[1-(Benzyloxy)but-3-en-2-yl](trimethyl)stannane;DTXSID70526742

Chemical Property of [1-(Benzyloxy)but-3-en-2-yl](trimethyl)stannane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 326.069268
• Heavy Atom Count: 16
• Complexity: 201

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Sn](C)(C)C(COCC1=CC=CC=C1)C=C

Technology Process of [1-(Benzyloxy)but-3-en-2-yl](trimethyl)stannane

There total 4 articles about [1-(Benzyloxy)but-3-en-2-yl](trimethyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Li(1+)*Cu(1+)*2Sn(CH3)3(1-)=[((CH3)3Sn)2Cu]Li + ((Z)-3-Bromo-allyloxymethyl)-benzene → (1-Benzyloxymethyl-allyl)-trimethyl-stannane (89358-34-9) + ((E)-4-Benzyloxy-but-2-enyl)-trimethyl-stannane (89358-41-8)

Guidance literature:

In tetrahydrofuran; -30°C; distn. (total yield 98 %);

DOI:10.1039/c39830001264

Reference yield:

[Me3SnCuC.tplbond.CC(Me)2OMe]Li + 1-[((E)-3-bromoallyloxy)methyl]benzene (610272-48-5) → (1-Benzyloxymethyl-allyl)-trimethyl-stannane (89358-34-9) + ((Z)-4-Benzyloxy-but-2-enyl)-trimethyl-stannane (89358-38-3)

Guidance literature:

In tetrahydrofuran; -30°C; distn. (total yield 24 %);

DOI:10.1039/c39830001264

Reference yield:

Li(1+)*Cu(1+)*2Sn(CH3)3(1-)=[((CH3)3Sn)2Cu]Li + 1-[((E)-3-bromoallyloxy)methyl]benzene (610272-48-5) → (1-Benzyloxymethyl-allyl)-trimethyl-stannane (89358-34-9) + ((Z)-4-Benzyloxy-but-2-enyl)-trimethyl-stannane (89358-38-3)

Guidance literature:

In tetrahydrofuran; -30°C; distn. (total yield 61 %);

DOI:10.1039/c39830001264

upstream raw materials:

1-[((E)-3-bromoallyloxy)methyl]benzene

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