4-Phenylcyclohexane-1-oneoxime

Base Information

• Chemical Name: 4-Phenylcyclohexane-1-oneoxime
• CAS No.: 4500-20-3
• Molecular Formula: C12H15NO
• Molecular Weight: 189.257
• Hs Code.: 2928000090
• Mol file: 4500-20-3.mol

Synonyms:4-Phenylcyclohexanone oxime;

Chemical Property of 4-Phenylcyclohexane-1-oneoxime

Chemical Property:

• Vapor Pressure: 3.48E-05mmHg at 25°C
• Boiling Point: 339.8°Cat760mmHg
• Flash Point: 210.7°C
• PSA: 32.59000
• Density: 1.1g/cm³
• LogP: 3.17440

Purity/Quality:

98%min ^*data from raw suppliers

4-phenylcyclohexanoneoxime ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Phenylcyclohexane-1-oneoxime

There total 5 articles about 4-Phenylcyclohexane-1-oneoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-phenyl-4-cyclohexanone (4894-75-1) → 4-phenylcyclohexanone oxime (4500-20-3)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; at 50 - 60 ℃; for 0.25h;

DOI:10.1002/jccs.201200011

Reference yield: 99.0%

→ 4-phenylcyclohexanone oxime (4500-20-3)

Guidance literature:

Reference yield: 83.0%

4-phenyl-cyclohexanol (5769-13-1,7335-12-8,5437-46-7) → 4-phenylcyclohexanone oxime (4500-20-3)

Guidance literature:

4-phenyl-cyclohexanol; With chromium(VI) oxide; aluminum oxide; tert-butyl alcohol; for 0.166667h;

With hydroxylamine hydrochloride; for 0.116667h;

DOI:10.1080/10426500490466535

upstream raw materials:

1-phenyl-4-cyclohexanone

4-phenyl-cyclohexanol

Downstream raw materials:

5-phenylazepan-2-one

N-(4-Phenyl-cyclohexyl)-hydroxylamine

cis-Benzoylamino-4-phenyl-cyclohexan

N-(trans-4-phenyl-cyclohexyl)-benzamide

Refernces

• 1、 -. "Process for preparing 4-phenyl cycloheptylamine". Paragraph 0017-0018. . Retrieved 2018/12/13.
• 2、 Liu, Zhao-Jing,Lu, Xi,Wang, Guan,Li, Lei,Jiang, Wei-Tao,Wang, Yu-Dong,Xiao, Bin,Fu, Yao. "Directing Group in Decarboxylative Cross-Coupling: Copper-Catalyzed Site-Selective C-N Bond Formation from Nonactivated Aliphatic Carboxylic Acids". supporting information. p. 9714 - 9719. Retrieved 2016/08/11.