Quinoline, 1-(4-bromophenyl)-1,5,6,7-tetrahydro-2,4-diphenyl-

Base Information

Chemical Name:Quinoline, 1-(4-bromophenyl)-1,5,6,7-tetrahydro-2,4-diphenyl-
CAS No.:89409-13-2
Molecular Formula:C27H22BrN
Molecular Weight:440.382
Hs Code.:
DSSTox Substance ID:DTXSID00392790
Wikidata:Q82191202

Synonyms:89409-13-2;Quinoline, 1-(4-bromophenyl)-1,5,6,7-tetrahydro-2,4-diphenyl-;DTXSID00392790

Suppliers and Price of Quinoline, 1-(4-bromophenyl)-1,5,6,7-tetrahydro-2,4-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Quinoline, 1-(4-bromophenyl)-1,5,6,7-tetrahydro-2,4-diphenyl-

Chemical Property:

XLogP3:7.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:439.09356
Heavy Atom Count:29
Complexity:667

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC=C2C(=C(C=C(N2C3=CC=C(C=C3)Br)C4=CC=CC=C4)C5=CC=CC=C5)C1

Technology Process of Quinoline, 1-(4-bromophenyl)-1,5,6,7-tetrahydro-2,4-diphenyl-

There total 1 articles about Quinoline, 1-(4-bromophenyl)-1,5,6,7-tetrahydro-2,4-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89409-06-3
Trifluoro-methanesulfonate1-(4-bromo-phenyl)-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium;

: 89409-13-2
1-(4-Bromo-phenyl)-2,4-diphenyl-1,5,6,7-tetrahydro-quinoline

Guidance literature:: With sodium hydride; In ethanol; at 25 ℃; for 0.25h;
DOI:10.1039/P19830002601

Reference yield: 77.0%

: 89409-13-2
1-(4-Bromo-phenyl)-2,4-diphenyl-1,5,6,7-tetrahydro-quinoline

: 1-(4-Bromo-phenyl)-8-[(E)-hydroxyimino]-2,4-diphenyl-5,6,7,8-tetrahydro-quinolinium; perchlorate

Guidance literature:: With sodium perchlorate; nitrosylchloride; In diethyl ether; ethanol;

Reference yield:

: 89409-13-2
1-(4-Bromo-phenyl)-2,4-diphenyl-1,5,6,7-tetrahydro-quinoline

: 8-benzoyl-2,4-diphenyl-5,6,7,8-tetrahydroquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 0.33 h / 25 °C

2: sodium hydride / ethanol / 0.33 h

3: 79 percent / dimethylformamide / 18 h / Heating

4: 1.) conc. hydrochloric acid, 2.) aq. sodium hydroxide / 1.) acetic acid, reflux, 10 min, 2.) 5 deg C

With hydrogenchloride; sodium hydroxide; sodium hydride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1039/P19830002601