Phosphonium, [oxybis[(5-cyano-2,1-phenylene)methylene]]bis[triphenyl-, dibromide

Base Information

Chemical Name:Phosphonium, [oxybis[(5-cyano-2,1-phenylene)methylene]]bis[triphenyl-, dibromide
CAS No.:89446-91-3
Molecular Formula:2Br*C₅₂H₄₀N₂OP₂
Molecular Weight:930.658
Hs Code.:

Synonyms:

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Chemical Property of Phosphonium, [oxybis[(5-cyano-2,1-phenylene)methylene]]bis[triphenyl-, dibromide

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Technology Process of Phosphonium, [oxybis[(5-cyano-2,1-phenylene)methylene]]bis[triphenyl-, dibromide

There total 4 articles about Phosphonium, [oxybis[(5-cyano-2,1-phenylene)methylene]]bis[triphenyl-, dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4731-34-4
2,2'-dimethyldiphenyl ether

: 89446-91-3
C₅₂H₄₀N₂OP₂⁽²⁺⁾*2Br^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / bromine / acetic acid / 0 °C

2: 79 percent / pyridine / 42 h / 230 °C / 1.) dry pyridine, 230 deg C, 42 h, 2.) ice, liquor ammonia, 3 h

3: 77 percent / NBS, dibenzoyl peroxide / CCl₄ / 36 h / Heating; Irradiation

4: dimethylformamide / 8 h / 160 °C

With N-Bromosuccinimide; bromine; dibenzoyl peroxide; In pyridine; tetrachloromethane; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 19209-61-1
4,4'-dibromo-2,2'-dimethyldiphenyl ether

: 89446-91-3
C₅₂H₄₀N₂OP₂⁽²⁺⁾*2Br^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / pyridine / 42 h / 230 °C / 1.) dry pyridine, 230 deg C, 42 h, 2.) ice, liquor ammonia, 3 h

2: 77 percent / NBS, dibenzoyl peroxide / CCl₄ / 36 h / Heating; Irradiation

3: dimethylformamide / 8 h / 160 °C

With N-Bromosuccinimide; dibenzoyl peroxide; In pyridine; tetrachloromethane; N,N-dimethyl-formamide;

Reference yield:

: 89446-88-8
4,4'-dicyano-2,2'-dimethyldiphenyl ether

: 89446-91-3
C₅₂H₄₀N₂OP₂⁽²⁺⁾*2Br^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / NBS, dibenzoyl peroxide / CCl₄ / 36 h / Heating; Irradiation

2: dimethylformamide / 8 h / 160 °C

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide;