Benzenepropanol, a-(1-nitroethyl)-

Base Information

Chemical Name:Benzenepropanol, a-(1-nitroethyl)-
CAS No.:89449-82-1
Molecular Formula:C11H15NO3
Molecular Weight:209.245
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanol, a-(1-nitroethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanol, a-(1-nitroethyl)-

There total 7 articles about Benzenepropanol, a-(1-nitroethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 104-53-0
3-phenyl-propionaldehyde

: 79-24-3
Nitroethane

: 89449-82-1,141377-58-4,138668-13-0,141377-57-3
4-nitro-1-phenyl-3-pentanol

Guidance literature:: With sodium hydroxide; cetyltrimethylammonium chloride; for 2h; Ambient temperature;
DOI:10.1021/jo961201h

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 79-24-3
Nitroethane

: 89449-82-1,141377-58-4,138668-13-0,141377-57-3
4-nitro-1-phenyl-3-pentanol

: 141377-58-4,138668-13-0,141377-57-3
(3S,4S)-4-nitro-1-phenylpentan-3-ol

Guidance literature:: With C₄₀H₃₄CuNO₅; In ethanol; at 20 ℃; for 72h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.01.026

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 79-24-3
Nitroethane

: 89449-82-1,141377-58-4,138668-13-0,141377-57-3
(3RS,4RS)-4-nitro-1-phenylpentan-3-ol

: 141377-58-4,138668-13-0,141377-57-3
(3S,4R)-4-nitro-1-phenylpentan-3-ol

: 141377-58-4,138668-13-0,141377-57-3
(3R,4S)-4-nitro-1-phenylpentan-3-ol

Guidance literature:: With C₁₉H₂₀F₂N₂O₄; neodymium(III) chloride hexahydrate; sodium t-butanolate; In 1,2-dimethoxyethane; at -40 ℃; for 20h; Reagent/catalyst; Overall yield = 94 %; stereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1016/j.tetlet.2016.03.041