1-{1-Bromo-2-[(oct-2-yn-1-yl)oxy]ethanesulfonyl}-4-methylbenzene

Base Information

Chemical Name:1-{1-Bromo-2-[(oct-2-yn-1-yl)oxy]ethanesulfonyl}-4-methylbenzene
CAS No.:89478-92-2
Molecular Formula:C17H23BrO3S
Molecular Weight:387.338
Hs Code.:
DSSTox Substance ID:DTXSID60527268

Synonyms:89478-92-2;DTXSID60527268;1-{1-Bromo-2-[(oct-2-yn-1-yl)oxy]ethanesulfonyl}-4-methylbenzene

Suppliers and Price of 1-{1-Bromo-2-[(oct-2-yn-1-yl)oxy]ethanesulfonyl}-4-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-{1-Bromo-2-[(oct-2-yn-1-yl)oxy]ethanesulfonyl}-4-methylbenzene

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:8
Exact Mass:386.05513
Heavy Atom Count:22
Complexity:461

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC#CCOCC(S(=O)(=O)C1=CC=C(C=C1)C)Br

Technology Process of 1-{1-Bromo-2-[(oct-2-yn-1-yl)oxy]ethanesulfonyl}-4-methylbenzene

There total 3 articles about 1-{1-Bromo-2-[(oct-2-yn-1-yl)oxy]ethanesulfonyl}-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 20739-58-6
2-octyn-1-ol

: 89478-86-4
1-bromovinyl p-tolyl sulphone

: 89478-92-2
1-(1-Bromo-2-oct-2-ynyloxy-ethanesulfonyl)-4-methyl-benzene

Guidance literature:: With sodium hydride; for 5h; Ambient temperature;

Reference yield:

: 5535-52-4
tolyl vinyl sulfone

: 89478-92-2
1-(1-Bromo-2-oct-2-ynyloxy-ethanesulfonyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / bromine / CCl₄ / 24 h / Ambient temperature

2: 70 percent / triethylamine / CH₂Cl₂ / 3.5 h

3: 93 percent / sodium hydride / 5 h / Ambient temperature

With bromine; sodium hydride; triethylamine; In tetrachloromethane; dichloromethane;

Reference yield:

: 59336-76-4
1,2-dibromo-1-p-tolylsulphonylethane

: 89478-92-2
1-(1-Bromo-2-oct-2-ynyloxy-ethanesulfonyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / triethylamine / CH₂Cl₂ / 3.5 h

2: 93 percent / sodium hydride / 5 h / Ambient temperature

With sodium hydride; triethylamine; In dichloromethane;