N-[(4-methylphenyl)sulfonyl]-Benzenesulfonimidoyl fluoride

Base Information

Chemical Name:N-[(4-methylphenyl)sulfonyl]-Benzenesulfonimidoyl fluoride
CAS No.:89538-93-2
Molecular Formula:C₁₃H₁₂FNO₃S₂
Molecular Weight:313.374
Hs Code.:
DSSTox Substance ID:DTXSID60529489

Synonyms:89538-93-2;N-[(4-methylphenyl)sulfonyl]- Benzenesulfonimidoyl fluoride;N-Tosylbenzenesulfonimidoyl fluoride;SCHEMBL17318141;DTXSID60529489;N-(4-Methylbenzene-1-sulfonyl)benzenesulfonimidoyl fluoride

Suppliers and Price of N-[(4-methylphenyl)sulfonyl]-Benzenesulfonimidoyl fluoride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[(4-methylphenyl)sulfonyl]-Benzenesulfonimidoyl fluoride

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:313.02426375
Heavy Atom Count:20
Complexity:533

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N=S(=O)(C2=CC=CC=C2)F

Technology Process of N-[(4-methylphenyl)sulfonyl]-Benzenesulfonimidoyl fluoride

There total 6 articles about N-[(4-methylphenyl)sulfonyl]-Benzenesulfonimidoyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 89538-92-1
N-(4-methylbenzenesulfonyl) phenyl sulfonimidoyl chloride

: 89538-93-2,89538-95-4,89539-05-9
N-(4-methylbenzenesulfonyl) phenyl sulfonimidoyl fluoride

Guidance literature:: With potassium fluoride; 18-crown-6 ether; In acetonitrile; at 20 ℃; for 24.5h; Inert atmosphere;
DOI:10.1002/chem.201901176

Reference yield: 69.0%

: 89538-92-1
N-(4-methylbenzenesulfonyl) phenyl sulfonimidoyl chloride

: 89538-93-2,89538-95-4,89539-05-9
N-(4-methylbenzenesulfonyl) phenyl sulfonimidoyl fluoride

: C₂₀H₁₉N₂O₅S₃^(1-)*K⁽¹⁺⁾

Guidance literature:: With potassium fluoride; In water; at 110 - 120 ℃; for 1h;

Reference yield:

: 4972-29-6
benzenesulphinyl chloride

: 89538-93-2,89538-95-4,89539-05-9
N-(4-methylbenzenesulfonyl) phenyl sulfonimidoyl fluoride

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 3 h / 80 °C

2: potassium fluoride; 18-crown-6 ether / acetonitrile / 24.5 h / 20 °C / Inert atmosphere

With potassium fluoride; 18-crown-6 ether; In toluene; acetonitrile;
DOI:10.1002/chem.201901176