Physoperuvine

Base Information

Chemical Name:Physoperuvine
CAS No.:60723-27-5
Molecular Formula:C8H15NO
Molecular Weight:141.2108
Hs Code.:2933990090
DSSTox Substance ID:DTXSID80332038
Wikidata:Q27107889
Metabolomics Workbench ID:69591
Mol file:60723-27-5.mol

Synonyms:physoperuvine

Suppliers and Price of Physoperuvine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
Physoperuvine ≥98%
5mg
$ 268.00

Total 2 raw suppliers

Chemical Property of Physoperuvine

Chemical Property:

Vapor Pressure:0.061mmHg at 25°C
Boiling Point:205°Cat760mmHg
Flash Point:69.6°C
PSA：23.47000
Density:1.122g/cm³
LogP:0.89100
XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:141.115364102
Heavy Atom Count:10
Complexity:148

Purity/Quality:

98% ^*data from raw suppliers

Physoperuvine ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2CCCC1(CC2)O
Description A novel alkaloid possessing a cyc1oheptanone structure, physoperuvine occurs in the roots of Physalis peruviana Linn. The structure is based upon chemical and spectroscopic evidence.

Technology Process of Physoperuvine

There total 5 articles about Physoperuvine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1180001-75-5
(1S)-1-[tert-butoxycarbonyl(methyl)amino]cycloheptan-4-one

: 60723-27-5
(+)-physoperuvine

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/b907341h

Reference yield:

: 181053-51-0
(5R)-5-(N-benzyloxycarbonyl-N-methyl)amino-2-cyclohepten-1-one

: 60723-27-5
(+)-physoperuvine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 1551.4 Torr; Yield given;
DOI:10.1139/v97-091

Reference yield:

: 157196-74-2
5-(N-benzyloxycarbonyl-N-methyl)amino-2-cyclohepten-1-one

: 60723-27-5
(+)-physoperuvine

Guidance literature:: Multi-step reaction with 4 steps

1: 30percent aq. H₂O₂, aq. KOH / tetrahydrofuran / -10 - 20 °C

2: hydrazine, 3 Angstroem molecular sieves, glacial AcOH / methanol / 2 h / Ambient temperature

3: PDC / CH₂Cl₂ / 12 h / Ambient temperature

4: H₂ / 30percent Pd/C / methanol / 2 h / 1551.4 Torr

With potassium hydroxide; dipyridinium dichromate; 3 A molecular sieve; hydrogen; dihydrogen peroxide; acetic acid; hydrazine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1139/v97-091