Benzamide, N-[2-[[4-(acetyloxy)-2-methylene-1-pyrrolidinyl]carbonyl]-4-methoxy-5-[[( 4-methylphenyl)sulfonyl]oxy]phenyl]-, (R)-

Base Information

Chemical Name:Benzamide, N-[2-[[4-(acetyloxy)-2-methylene-1-pyrrolidinyl]carbonyl]-4-methoxy-5-[[( 4-methylphenyl)sulfonyl]oxy]phenyl]-, (R)-
CAS No.:89625-56-9
Molecular Formula:C₂₉H₂₈N₂O₈S
Molecular Weight:564.616
Hs Code.:

Synonyms:

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Chemical Property of Benzamide, N-[2-[[4-(acetyloxy)-2-methylene-1-pyrrolidinyl]carbonyl]-4-methoxy-5-[[( 4-methylphenyl)sulfonyl]oxy]phenyl]-, (R)-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzamide, N-[2-[[4-(acetyloxy)-2-methylene-1-pyrrolidinyl]carbonyl]-4-methoxy-5-[[( 4-methylphenyl)sulfonyl]oxy]phenyl]-, (R)-

There total 16 articles about Benzamide, N-[2-[[4-(acetyloxy)-2-methylene-1-pyrrolidinyl]carbonyl]-4-methoxy-5-[[( 4-methylphenyl)sulfonyl]oxy]phenyl]-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 89625-56-9
Acetic acid 1-[2-benzoylamino-5-methoxy-4-(toluene-4-sulfonyloxy)-benzoyl]-5-methylene-pyrrolidin-3-yl ester

Guidance literature:: Multi-step reaction with 11 steps

1: Ag₂O

2: HNO₂

3: 62 percent / H₂ / 10percent Pd/C

4: 83 percent

5: 65 percent

6: 83 percent / oxalyl chloride

7: benzene / 12 h / Heating

8: p-TsOH

10: KBr / dimethylsulfoxide

11: NaH / tetrahydrofuran

With oxalyl dichloride; hydrogen; cis-nitrous acid; sodium hydride; toluene-4-sulfonic acid; potassium bromide; silver(l) oxide; palladium on activated charcoal; In tetrahydrofuran; dimethyl sulfoxide; benzene;

Reference yield:

: 60547-92-4
4-(benzyloxy)-5-methoxy-2-nitrobenzoic acid

: 89625-56-9
Acetic acid 1-[2-benzoylamino-5-methoxy-4-(toluene-4-sulfonyloxy)-benzoyl]-5-methylene-pyrrolidin-3-yl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 62 percent / H₂ / 10percent Pd/C

2: 83 percent

3: 65 percent

4: 83 percent / oxalyl chloride

5: benzene / 12 h / Heating

6: p-TsOH

8: KBr / dimethylsulfoxide

9: NaH / tetrahydrofuran

With oxalyl dichloride; hydrogen; sodium hydride; toluene-4-sulfonic acid; potassium bromide; palladium on activated charcoal; In tetrahydrofuran; dimethyl sulfoxide; benzene;

Reference yield:

: 1486-53-9
4-(benzyloxy)-3-methoxybenzoic acid

: 89625-56-9
Acetic acid 1-[2-benzoylamino-5-methoxy-4-(toluene-4-sulfonyloxy)-benzoyl]-5-methylene-pyrrolidin-3-yl ester

Guidance literature:: Multi-step reaction with 10 steps

1: HNO₂

2: 62 percent / H₂ / 10percent Pd/C

3: 83 percent

4: 65 percent

5: 83 percent / oxalyl chloride

6: benzene / 12 h / Heating

7: p-TsOH

9: KBr / dimethylsulfoxide

10: NaH / tetrahydrofuran

With oxalyl dichloride; hydrogen; cis-nitrous acid; sodium hydride; toluene-4-sulfonic acid; potassium bromide; palladium on activated charcoal; In tetrahydrofuran; dimethyl sulfoxide; benzene;