2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine

Base Information

• Chemical Name: 2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine
• CAS No.: 30469-02-4
• Molecular Formula: C12H7 Cl N4 O
• Molecular Weight: 258.6632
• Mol file: 30469-02-4.mol

Synonyms:Imidazo[1,2-a]pyrimidine,2-(p-chlorophenyl)-3-nitroso- (8CI); NSC 77444

Chemical Property of 2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.5g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine

There total 3 articles about 2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobenzoylmethyl bromide (536-38-9) → 2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine (30469-02-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,2-dimethoxy-ethane / 48 h / Heating

2: sodium nitrite / acetic acid

With sodium nitrite; In 1,2-dimethoxyethane; acetic acid;

DOI:10.1248/cpb.40.1170

Reference yield:

2-(4-chlorophenyl)imidazol[1,2-a]pyrimidine (56921-86-9) → 2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine (30469-02-4)

Guidance literature:

With acetic acid; sodium nitrite;

DOI:10.1016/0223-5234(91)90208-5

Reference yield:

→ 2-(4-chlorophenyl)-3-nitrosoimidazo[1,2-a]pyrimidine (30469-02-4)

Guidance literature:

2-p-Chlorphenylimidazo<1,2-a>pyrimidin, NaNO2/Eg.;

upstream raw materials:

2-(4-chlorophenyl)imidazol[1,2-a]pyrimidine

4-chlorobenzoylmethyl bromide

Downstream raw materials:

3-(p-chlorobenzoyl)-5-amino-1,2,4-oxadiazole

2-(4-Chloro-phenyl)-3-nitro-imidazo[1,2-a]pyrimidine

2-(4-Chloro-phenyl)-imidazo[1,2-a]pyrimidin-3-ylamine

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