Ethyl 3-oxo-2-[(3-phenylacryloyl)amino]butanoate

Base Information

Chemical Name:Ethyl 3-oxo-2-[(3-phenylacryloyl)amino]butanoate
CAS No.:89723-84-2
Molecular Formula:C15H17NO4
Molecular Weight:275.304
Hs Code.:
DSSTox Substance ID:DTXSID70705898

Synonyms:89723-84-2;Ethyl 3-oxo-2-[(3-phenylacryloyl)amino]butanoate;DTXSID70705898;ethyl 2-cinnamoylaminoacetoacetate;BFPPTJUYWWJGKZ-UHFFFAOYSA-N

Suppliers and Price of Ethyl 3-oxo-2-[(3-phenylacryloyl)amino]butanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 3-oxo-2-[(3-phenylacryloyl)amino]butanoate

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:275.11575802
Heavy Atom Count:20
Complexity:383

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C(=O)C)NC(=O)C=CC1=CC=CC=C1

Technology Process of Ethyl 3-oxo-2-[(3-phenylacryloyl)amino]butanoate

There total 1 articles about Ethyl 3-oxo-2-[(3-phenylacryloyl)amino]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.9%

: 20207-16-3
ethyl 2-amino-3-oxobutanoate hydrochloride

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 89723-84-2
ethyl 2-cinnamoylaminoacetoacetate

Guidance literature:: With triethylamine; In chloroform; for 0.333333h; ice cooling;
DOI:10.1248/cpb.34.2840

Reference yield: 80.7%

: 89723-84-2
ethyl 2-cinnamoylaminoacetoacetate

: 89723-85-3
(E)-ethyl 5-methyl-2-styryloxazole-4-carboxylate

Guidance literature:: With trichlorophosphate; at 100 - 110 ℃; for 0.5h;
DOI:10.1248/cpb.34.2840

Reference yield:

: 89723-84-2
ethyl 2-cinnamoylaminoacetoacetate

: 89723-87-5
4-chloromethyl-5-methyl-2-[(E)-2-phenylethenyl]oxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 80.7 percent / POCl₃ / 0.5 h / 100 - 110 °C

2: 71.5 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 1 h / ice cooling

3: 90.7 percent / SOCl₂ / 0.5 h / Ambient temperature

With lithium aluminium tetrahydride; thionyl chloride; trichlorophosphate; In tetrahydrofuran; diethyl ether;
DOI:10.1248/cpb.34.2840