1,2,3,4-Tetra-tert-butyl-1,3,2,4-diazadiboretidine

Base Information

Chemical Name:1,2,3,4-Tetra-tert-butyl-1,3,2,4-diazadiboretidine
CAS No.:89787-00-8
Molecular Formula:C₁₆H₃₆B₂N₂
Molecular Weight:278.097
Hs Code.:
DSSTox Substance ID:DTXSID10553552
Wikidata:Q82434160

Synonyms:89787-00-8;1,2,3,4-Tetra-tert-butyl-1,3,2,4-diazadiboretidine;DTXSID10553552

Suppliers and Price of 1,2,3,4-Tetra-tert-butyl-1,3,2,4-diazadiboretidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,3,4-Tetra-tert-butyl-1,3,2,4-diazadiboretidine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:278.3064595
Heavy Atom Count:20
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B1(N(B(N1C(C)(C)C)C(C)(C)C)C(C)(C)C)C(C)(C)C

Technology Process of 1,2,3,4-Tetra-tert-butyl-1,3,2,4-diazadiboretidine

There total 1 articles about 1,2,3,4-Tetra-tert-butyl-1,3,2,4-diazadiboretidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110486-11-8
1,2,3,4-tetra-tert-butyl-4-(phenylethynyl)-1,3-diazonia-2,4-diboratacyclobutene

: 110472-71-4
tert-butyl(tert-butylamino)(phenylethynyl)borane

: 89787-00-8
1,3-di-t-butyl-2,4-di-t-butylamino-cyclo-1,3-diaza-2,4-diborane

Guidance literature:: heating to 220°C for 30 min; distn. at 80-95°C, 0.002 Torr yields a mixt. of the 2 products; (1)H, (11)B, (13)C NMR, MS; elem. anal.;

Reference yield: 80.0%

: 536-74-3
phenylacetylene

: 89787-00-8
1,3-di-t-butyl-2,4-di-t-butylamino-cyclo-1,3-diaza-2,4-diborane

: 110486-11-8
1,2,3,4-tetra-tert-butyl-4-(phenylethynyl)-1,3-diazonia-2,4-diboratacyclobutene

Guidance literature:: zinc(II) chloride; In dichloromethane; stirring for 4 h at room temp.; ZnCl2 filtered off and washed with CH2Cl2; volatile compounds removed in vac., residue dissolved in hexane; crystn. at -20°C; (1)H, (11)B, (13)C NMR spectroscopy, MS; elem. anal.;