3-Iodo-4-methoxybenzoyl chloride

Base Information

Chemical Name:3-Iodo-4-methoxybenzoyl chloride
CAS No.:89893-95-8
Molecular Formula:C8H6ClIO2
Molecular Weight:296.492
Hs Code.:
DSSTox Substance ID:DTXSID50474212
Nikkaji Number:J1.087.993K
Wikidata:Q82304061

Synonyms:3-Iodo-4-methoxybenzoyl chloride;4-Methoxy-3-iodobenzoyl chloride;89893-95-8;3-Iodo-p-anisoyl chloride;SCHEMBL6440090;DTXSID50474212;ZFSIGTASDSRLCO-UHFFFAOYSA-N;AKOS025123941

Suppliers and Price of 3-Iodo-4-methoxybenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-Iodo-4-methoxybenzoyl chloride

Chemical Property:

PSA：26.30000
LogP:2.67880
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:295.91010
Heavy Atom Count:12
Complexity:174

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(=O)Cl)I

Technology Process of 3-Iodo-4-methoxybenzoyl chloride

There total 3 articles about 3-Iodo-4-methoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.5%

: 68507-19-7
3-iodo-4-methoxybenzoic acid

: 89893-95-8
3-iodo-4-methoxybenzoyl chloride

Guidance literature:: With phosphorus pentachloride; In chloroform; for 1h; Heating;
DOI:10.1021/jo981186b

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 89893-95-8
3-iodo-4-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 65.2 percent / I₂, H₂SO₄, HNO₃ / acetic acid / 0.5 h / 50 °C

2: 85.5 percent / PCl₅ / CHCl₃ / 1 h / Heating

With phosphorus pentachloride; sulfuric acid; iodine; nitric acid; In chloroform; acetic acid;
DOI:10.1021/jo981186b

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 89893-95-8
3-iodo-4-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: I₂, aq. HNO₃, H₂SO₄, AcOH

2: PCl₅ / CHCl₃

With phosphorus pentachloride; sulfuric acid; iodine; nitric acid; acetic acid; In chloroform;