α-Methyl-2-phenanthreneacetic acid

Base Information

Chemical Name:α-Methyl-2-phenanthreneacetic acid
CAS No.:40452-14-0
Molecular Formula:C17H14O2
Molecular Weight:250.2919
Hs Code.:
Mol file:40452-14-0.mol

Synonyms:2-(2'-Phenanthryl)propionic acid;2-(2-phenanthryl)propanoic acid;Propionic acid,2-(2-phenanthryl);

Suppliers and Price of α-Methyl-2-phenanthreneacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-Methyl-2-phenanthreneacetic acid

Chemical Property:

Vapor Pressure:2.29E-09mmHg at 25°C
Boiling Point:462.9°Cat760mmHg
PKA:4.79±0.30(Predicted)
Flash Point:359.5°C
PSA：37.30000
Density:1.236g/cm³
LogP:4.18110

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of α-Methyl-2-phenanthreneacetic acid

There total 7 articles about α-Methyl-2-phenanthreneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 128479-19-6
2-(2-phenanthryl)propanenitrile

: 40452-14-0
2-(2'-Phenanthryl)propionic acid

Guidance literature:: With sulfuric acid; In water; acetic acid; for 2h; Heating;
DOI:10.1002/ardp.19903230412

Reference yield: 63.0%

: 74688-72-5
2-phenanthrylacetic acid

: 77-78-1
dimethyl sulfate

: 40452-14-0
2-(2'-Phenanthryl)propionic acid

: 138470-07-2
2-Methyl-2-phenanthren-2-yl-propionic acid

Guidance literature:: With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; for 8h; Yields of byproduct given; Heating;
DOI:10.1002/ardp.2503241206

Reference yield:

: 5960-69-0
2-acetylphenanthrene

: 40452-14-0
2-(2'-Phenanthryl)propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent Chromat_. / NaBH₄ / tetrahydrofuran; ethanol / 12 h / Ambient temperature

2: 95 percent / SOCl₂ / benzene / 4 h / Heating

3: 38 percent / dimethylsulfoxide / 7 h / 70 - 75 °C

4: 67 percent / H₂SO₄ / acetic acid; H₂O / 2 h / Heating

With sodium tetrahydroborate; thionyl chloride; sulfuric acid; In tetrahydrofuran; ethanol; water; acetic acid; dimethyl sulfoxide; benzene;
DOI:10.1002/ardp.19903230412