2,2'-(Ethane-1,2-diyl)bis(5-nitroaniline)

Base Information

Chemical Name:2,2'-(Ethane-1,2-diyl)bis(5-nitroaniline)
CAS No.:90018-60-3
Molecular Formula:C14H14N4O4
Molecular Weight:302.29
Hs Code.:
DSSTox Substance ID:DTXSID00525420
Wikidata:Q82393004

Synonyms:90018-60-3;2,2'-(Ethane-1,2-diyl)bis(5-nitroaniline);DTXSID00525420

Suppliers and Price of 2,2'-(Ethane-1,2-diyl)bis(5-nitroaniline)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-(Ethane-1,2-diyl)bis(5-nitroaniline)

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:302.10150494
Heavy Atom Count:22
Complexity:371

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1[N+](=O)[O-])N)CCC2=C(C=C(C=C2)[N+](=O)[O-])N

Technology Process of 2,2'-(Ethane-1,2-diyl)bis(5-nitroaniline)

There total 2 articles about 2,2'-(Ethane-1,2-diyl)bis(5-nitroaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 34124-14-6
2,2'-ethylenedianiline

: 90018-60-3
2,2'-diamino-4,4'-dinitrobibenzyl

Guidance literature:: With sulfuric acid; nitric acid; at 10 ℃; for 2h;
DOI:10.1016/S0040-4020(01)87932-1

Reference yield:

: 16968-19-7
2,2'-dinitrobibenzyl

: 90018-60-3
2,2'-diamino-4,4'-dinitrobibenzyl

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / hydrazine monohydrate / FeOOH / ethanol; N,N-dimethyl-acetamide / 3 h / Heating

2: 73 percent / fuming nitric acid, conc. sulfuric acid / 2 h / 10 °C

With sulfuric acid; nitric acid; hydrazine hydrate; hydrated iron(III) oxide; In ethanol; N,N-dimethyl acetamide;
DOI:10.1016/S0040-4020(01)87932-1