N,N'-Dioctylhexanediamide

Base Information

• Chemical Name: N,N'-Dioctylhexanediamide
• CAS No.: 37118-48-2
• Molecular Formula: C22H44N2O2
• Molecular Weight: 368.597
• Mol file: 37118-48-2.mol

Synonyms:N,N'-Dioctyladipic amide;N,N'-Dioctylhexanediamide;

Chemical Property of N,N'-Dioctylhexanediamide

Chemical Property:

• Boiling Point: 564°Cat760mmHg
• Flash Point: 153.2°C
• PSA: 58.20000
• Density: 0.913g/cm³
• LogP: 6.28200

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-Dioctylhexanediamide

There total 3 articles about N,N'-Dioctylhexanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

Adipic acid (124-04-9) + n-Octylamine (111-86-4) → N,N'-dioctyl-hexanediamide (37118-48-2)

Guidance literature:

Adipic acid; With thionyl chloride; triphenylphosphine; for 2h; Heating;

n-Octylamine; With triethylamine; In dichloromethane;

DOI:10.3390/90500278

Reference yield:

Adipic acid (124-04-9) → N,N'-dioctyl-hexanediamide (37118-48-2)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride; triphenyl phosphine / 2 h / Heating

2: 320 mg / triethylamine / CH₂Cl₂

With thionyl chloride; triethylamine; triphenylphosphine; In dichloromethane;

DOI:10.1021/jo0505369

Reference yield:

n-Octylamine (111-86-4) + Adipic acid dichloride (111-50-2) → N,N'-dioctyl-hexanediamide (37118-48-2)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1021/jo0505369

upstream raw materials:

Adipic acid

n-Octylamine

Adipic acid dichloride

Refernces

• 1、 Ballester, Pablo,Costa, Antoni,Deya, Pere M.,Frontera, Antonio,Gomila, Rosa M.,Oliva, Ana I.,Sanders, Jeremy K. M.,Hunter, Christopher A.. "Self-assembly, binding, and dynamic properties of heterodimeric porphyrin macrocycles". . p. 6616 - 6622. Retrieved 2007/10/03.