2,5-Pyrrolidinedione, 1-[2-(bromomethyl)-4-methoxy-5-methylphenyl]-

Base Information

Chemical Name:2,5-Pyrrolidinedione, 1-[2-(bromomethyl)-4-methoxy-5-methylphenyl]-
CAS No.:90173-79-8
Molecular Formula:C13H14BrNO3
Molecular Weight:312.15900
Hs Code.:

Synonyms:2,5-Pyrrolidinedione,1-[2-(bromomethyl)-4-methoxy-5-methylphenyl];N-(2-Brommethyl-4-methoxy-5-methylphenyl)succinimid;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Pyrrolidinedione, 1-[2-(bromomethyl)-4-methoxy-5-methylphenyl]-

Chemical Property:

PSA：46.61000
LogP:2.61690

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,5-Pyrrolidinedione, 1-[2-(bromomethyl)-4-methoxy-5-methylphenyl]-

There total 2 articles about 2,5-Pyrrolidinedione, 1-[2-(bromomethyl)-4-methoxy-5-methylphenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 90163-05-6
N-(2-Hydroxymethyl-4-methoxy-5-methylphenyl)succinimid

: 90173-79-8
N-(2-Brommethyl-4-methoxy-5-methylphenyl)succinimid

Guidance literature:: With dibromohexachloroethane; triphenylphosphine; In 1,2-dichloro-ethane; at -20 - -18 ℃; for 2.5h;
DOI:10.1002/jlac.198519850712

Reference yield:

: 90163-04-5
N-(2-Formyl-4-methoxy-5-methylphenyl)succinimid

: 90173-79-8
N-(2-Brommethyl-4-methoxy-5-methylphenyl)succinimid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 0,1percent methylorange, NaBH₃CN / tetrahydrofuran; H₂O / 1 h

2: 97 percent / triphenylphosphane, dibromohexachloroethane / 1,2-dichloro-ethane / 2.5 h / -20 - -18 °C

With dibromohexachloroethane; methyl orange; sodium cyanoborohydride; triphenylphosphine; In tetrahydrofuran; water; 1,2-dichloro-ethane;
DOI:10.1002/jlac.198519850712