2,6-Dimethoxy-3-methyl-9H-carbazole

Base Information

• Chemical Name: 2,6-Dimethoxy-3-methyl-9H-carbazole
• CAS No.: 29093-41-2
• Molecular Formula: C₁₅H₁₅NO₂
• Molecular Weight: 241.29
• Hs Code.: 2933990090
• DSSTox Substance ID: DTXSID70183339
• Nikkaji Number: J976.635I
• Wikidata: Q83054097
• Metabolomics Workbench ID: 136348
• ChEMBL ID: CHEMBL463555
• Mol file: 29093-41-2.mol

Synonyms:Glycozolidine;2,6-Dimethoxy-3-methyl-9H-carbazole;29093-41-2;9H-Carbazole, 2,6-dimethoxy-3-methyl-;CHEMBL463555;SCHEMBL15203441;2,6-dimethoxy-3-methylcarbazole;DTXSID70183339

Chemical Property of 2,6-Dimethoxy-3-methyl-9H-carbazole

Chemical Property:

• Vapor Pressure: 2.75E-07mmHg at 25°C
• Boiling Point: 432.7°Cat760mmHg
• Flash Point: 155.9°C
• PSA: 34.25000
• Density: 1.204g/cm³
• LogP: 3.64670
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 241.110278721
• Heavy Atom Count: 18
• Complexity: 296

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC2=C(C=C1OC)NC3=C2C=C(C=C3)OC

Technology Process of 2,6-Dimethoxy-3-methyl-9H-carbazole

There total 21 articles about 2,6-Dimethoxy-3-methyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(3'-Chloro-5,4'-dimethoxy-5'-methyl-biphenyl-2-yl)-carbamic acid tert-butyl ester (151692-25-0) → 2,6-dimethoxy-3-methylcarbazole (29093-41-2)

Guidance literature:

With potassium amide; In ammonia; at -33 ℃; for 3h;

DOI:10.3987/COM-93-6368

Reference yield: 80.0%

3-methoxy-N-(4-methoxyphenyl)-4-methylaniline (36661-35-5) → 2,6-dimethoxy-3-methylcarbazole (29093-41-2)

Guidance literature:

With copper diacetate; palladium diacetate; In N,N-dimethyl-formamide; at 130 ℃; for 1h; Sealed tube; Microwave irradiation;

DOI:10.1002/ejoc.200900537

Reference yield: 65.0%

methyl 2,6-dimethoxy-9H-carbazole-3-carboxylate → 2,6-dimethoxy-3-methylcarbazole (29093-41-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 65 ℃; for 1h;

DOI:10.1039/c3ra44903c

upstream raw materials:

diazomethane

6-hydroxy-2-methoxy-3-methyl-9H-carbazole

(3'-Chloro-5,4'-dimethoxy-5'-methyl-biphenyl-2-yl)-carbamic acid tert-butyl ester

2-chloro-5-methoxy-4-methyl-N-(4-methoxyphenyl)aniline

Downstream raw materials:

glycozolidal

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