3-Quinolinecarboxylic acid, 7-(cyclohexylamino)-6-fluoro-1,4-dihydro-1-[1-methyl-2-[(tetrahydro-2H- pyran-2-yl)oxy]ethyl]-4-oxo-, ethyl ester

Base Information

• Chemical Name: 3-Quinolinecarboxylic acid, 7-(cyclohexylamino)-6-fluoro-1,4-dihydro-1-[1-methyl-2-[(tetrahydro-2H- pyran-2-yl)oxy]ethyl]-4-oxo-, ethyl ester
• CAS No.: 902121-27-1
• Molecular Formula: C26H35FN2O5
• Molecular Weight: 474.573

Synonyms:

Chemical Property of 3-Quinolinecarboxylic acid, 7-(cyclohexylamino)-6-fluoro-1,4-dihydro-1-[1-methyl-2-[(tetrahydro-2H- pyran-2-yl)oxy]ethyl]-4-oxo-, ethyl ester

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 3-Quinolinecarboxylic acid, 7-(cyclohexylamino)-6-fluoro-1,4-dihydro-1-[1-methyl-2-[(tetrahydro-2H- pyran-2-yl)oxy]ethyl]-4-oxo-, ethyl ester

There total 1 articles about 3-Quinolinecarboxylic acid, 7-(cyclohexylamino)-6-fluoro-1,4-dihydro-1-[1-methyl-2-[(tetrahydro-2H- pyran-2-yl)oxy]ethyl]-4-oxo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) + ethyl 7-(cyclohexylamino)-6-fluoro-1-(2-hydroxy-1-methylethyl)-4-oxo-1,4-dihydroquinoline-3-carboxylate (836620-92-9) → ethyl 7-(cyclohexylamino)-6-fluoro-1-[1-methyl-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]-4-oxo-1,4-dihydroquinoline-3-carboxylate (902121-27-1)

Guidance literature:

With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃;

Reference yield:

ethyl 7-(cyclohexylamino)-6-fluoro-1-[1-methyl-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]-4-oxo-1,4-dihydroquinoline-3-carboxylate (902121-27-1) → 7-(cyclohexylamino)-6-fluoro-1-[1-methyl-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]-4-oxo-1,4-dihydroquinoline-3-carboxylic acid (836621-62-6)

Guidance literature:

With sodium hydroxide; ethanol; water; In tetrahydrofuran;

upstream raw materials:

3,4-dihydro-2H-pyran

ethyl 7-(cyclohexylamino)-6-fluoro-1-(2-hydroxy-1-methylethyl)-4-oxo-1,4-dihydroquinoline-3-carboxylate

Downstream raw materials:

7-(cyclohexylamino)-6-fluoro-1-[1-methyl-2-(tetrahydro-2H-pyran-2-yloxy)ethyl]-4-oxo-1,4-dihydroquinoline-3-carboxylic acid

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