N-[4-(Diphenylphosphoryl)buta-1,3-diyn-1-yl]-N-methylaniline

Base Information

Chemical Name:N-[4-(Diphenylphosphoryl)buta-1,3-diyn-1-yl]-N-methylaniline
CAS No.:90235-51-1
Molecular Formula:C₂₃H₁₈NOP
Molecular Weight:355.376
Hs Code.:
DSSTox Substance ID:DTXSID20530450
Wikidata:Q82401579

Synonyms:90235-51-1;DTXSID20530450;N-[4-(Diphenylphosphoryl)buta-1,3-diyn-1-yl]-N-methylaniline

Suppliers and Price of N-[4-(Diphenylphosphoryl)buta-1,3-diyn-1-yl]-N-methylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[4-(Diphenylphosphoryl)buta-1,3-diyn-1-yl]-N-methylaniline

Chemical Property:

XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:355.112601195
Heavy Atom Count:26
Complexity:602

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C#CC#CP(=O)(C1=CC=CC=C1)C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of N-[4-(Diphenylphosphoryl)buta-1,3-diyn-1-yl]-N-methylaniline

There total 4 articles about N-[4-(Diphenylphosphoryl)buta-1,3-diyn-1-yl]-N-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 82505-84-8
N-<4-(Diphenylphosphino)-1,3-butadiinyl>-N-methyl-anilin

: 90235-51-1
<4-(Methylphenylamino)-1,3-butadiinyl>diphenylphosphanoxid

Guidance literature:: With dihydrogen peroxide; In acetone; for 0.166667h; Ambient temperature;

Reference yield:

: 82505-76-8
(3,4,4-Trichloro-N-methyl-N-phenyl-3-buten-1-inyl)amin

: 90235-51-1
<4-(Methylphenylamino)-1,3-butadiinyl>diphenylphosphanoxid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.6 N LiBu / diethyl ether; hexane / 1.5 h / Ambient temperature

2: 50 percent / diethyl ether / 4 h / Ambient temperature

3: 67 percent / 30percent H₂O₂ / acetone / 0.17 h / Ambient temperature

With n-butyllithium; dihydrogen peroxide; In diethyl ether; hexane; acetone;

Reference yield:

: 35954-01-9
lithium N-methylanilide

: 90235-51-1
<4-(Methylphenylamino)-1,3-butadiinyl>diphenylphosphanoxid

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent

2: 1.6 N LiBu / diethyl ether; hexane / 1.5 h / Ambient temperature

3: 50 percent / diethyl ether / 4 h / Ambient temperature

4: 67 percent / 30percent H₂O₂ / acetone / 0.17 h / Ambient temperature

With n-butyllithium; dihydrogen peroxide; In diethyl ether; hexane; acetone;