Technology Process of Benz(a)anthracen-8-ol, 7,12-dimethyl-
There total 9 articles about Benz(a)anthracen-8-ol, 7,12-dimethyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron tribromide;
In
benzene;
for 0.75h;
Heating;
deoxygenated solvents;
DOI:10.1021/jo01300a007
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dimethyl sulfoxide, sodium hydride
2: LiAlH4 / tetrahydrofuran / 2 h / cooling
3: 96 percent / HCl, SnCl2
4: 84 percent / BBr3 / benzene / 0.75 h / Heating; deoxygenated solvents
With
hydrogenchloride; lithium aluminium tetrahydride; boron tribromide; sodium hydride; dimethyl sulfoxide; tin(ll) chloride;
In
tetrahydrofuran; benzene;
DOI:10.1021/jo01300a007
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) acetic anhydride, zinc chloride, 2.) potassium dichromate / 1.) reflux, acetic acid, 2 h, 2.) +H2O, reflux, 1 h
2: dimethyl sulfoxide, sodium hydride
3: LiAlH4 / tetrahydrofuran / 2 h / cooling
4: 96 percent / HCl, SnCl2
5: 84 percent / BBr3 / benzene / 0.75 h / Heating; deoxygenated solvents
With
hydrogenchloride; potassium dichromate; lithium aluminium tetrahydride; acetic anhydride; boron tribromide; sodium hydride; dimethyl sulfoxide; tin(ll) chloride; zinc(II) chloride;
In
tetrahydrofuran; benzene;
DOI:10.1021/jo01300a007
