Benzamide, 4-methyl-N-(1,2,2-trichloroethyl)-

Base Information

Chemical Name:Benzamide, 4-methyl-N-(1,2,2-trichloroethyl)-
CAS No.:90283-59-3
Molecular Formula:C10H10Cl3NO
Molecular Weight:266.554
Hs Code.:
DSSTox Substance ID:DTXSID10462019

Synonyms:90283-59-3;Benzamide, 4-methyl-N-(1,2,2-trichloroethyl)-;p-toluic acid N-(1,2,2-trichloroethyl)amide;DTXSID10462019

Suppliers and Price of Benzamide, 4-methyl-N-(1,2,2-trichloroethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzamide, 4-methyl-N-(1,2,2-trichloroethyl)-

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:264.982797
Heavy Atom Count:15
Complexity:215

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)NC(C(Cl)Cl)Cl

Technology Process of Benzamide, 4-methyl-N-(1,2,2-trichloroethyl)-

There total 3 articles about Benzamide, 4-methyl-N-(1,2,2-trichloroethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 90283-58-2
N-(2,2-Dichloro-1-hydroxy-ethyl)-4-methyl-benzamide

: 90283-59-3
p-toluic acid N-(1,2,2-trichloroethyl)amide

Guidance literature:: With thionyl chloride; at 40 - 50 ℃; for 1h;

Reference yield:

: 54888-30-1
N-(2,2-dichlorovinyl)-4-methylbenzamide

: 90283-59-3
p-toluic acid N-(1,2,2-trichloroethyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / 25percent ammonium hydroxide / dioxane / 70 h / 20 - 25 °C

2: 85 percent / NaNO₂, conc. HCl / H₂O / 24 h / 20 - 25 °C

3: 91 percent / SOCl₂ / 1 h / 40 - 50 °C

With hydrogenchloride; ammonium hydroxide; thionyl chloride; sodium nitrite; In 1,4-dioxane; water;

Reference yield:

: 90283-56-0
N-(1-Amino-2,2-dichloro-ethyl)-4-methyl-benzamide

: 90283-59-3
p-toluic acid N-(1,2,2-trichloroethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaNO₂, conc. HCl / H₂O / 24 h / 20 - 25 °C

2: 91 percent / SOCl₂ / 1 h / 40 - 50 °C

With hydrogenchloride; thionyl chloride; sodium nitrite; In water;