Benzene, (2-methyl-1-octenyl)-, (Z)-

Base Information

Chemical Name:Benzene, (2-methyl-1-octenyl)-, (Z)-
CAS No.:90334-47-7
Molecular Formula:C₁₅H₂₂
Molecular Weight:202.34
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, (2-methyl-1-octenyl)-, (Z)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, (2-methyl-1-octenyl)-, (Z)-

There total 5 articles about Benzene, (2-methyl-1-octenyl)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1507-88-6,55131-21-0
<(E)-3-chloro-2-methyl-1-propenyl>benzene

: 6393-56-2
pentylmagnesium chloride

: (+)-2-methyl-3-phenyl-1-octene

: 84530-49-4,90334-47-7
2-methyl-1-phenyloct-1-ene

Guidance literature:: <(E)-3-chloro-2-methyl-1-propenyl>benzene; With O,O'-(S)-(1,1'-dinaphthyl-2,2'-diyl)-N,N-di-(S,S)-[2-phenylethylphosphoramidite]; copper(I) thiophene-2-carboxylate; In dichloromethane; at 20 ℃; Inert atmosphere;

pentylmagnesium chloride; In diethyl ether; dichloromethane; at -78 ℃; for 5h; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/adsc.200800086

Reference yield:

: 7695-69-4
bis(phenylthio)methylbenzene

: 111-13-7
hexyl-methyl-ketone

: 84530-49-4,90334-47-7
2-methyl-1-phenyloct-1-ene

Guidance literature:: With titanocene(II) triethylphosphite complex; Yield given. Multistep reaction; 1.) THF, room temperature, 5 min, 2.) room temperature, 30 min;
DOI:10.1021/ja962240d

Reference yield:

: 111-13-7
hexyl-methyl-ketone

: 84530-49-4,90334-47-7
2-methyl-1-phenyloct-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: HCOONa / methanol; H₂O

2: 1) MeLi, 2) NEt₃, PCl₃ / 1) THF, -40 deg C to -25 deg C, 2) THF, -78 deg C to 20 deg C

With methyllithium; sodium formate; triethylamine; phosphorus trichloride; In methanol; water;
DOI:10.1039/c39840000022