Methanesulfonamide, N-[5-[2-[[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-2H-3,1-benzoxazin-1(4H)-yl )propyl]amino]-1-hydroxyethyl]-2-(phenylmethoxy)phenyl]-

Base Information

Chemical Name:Methanesulfonamide, N-[5-[2-[[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-2H-3,1-benzoxazin-1(4H)-yl )propyl]amino]-1-hydroxyethyl]-2-(phenylmethoxy)phenyl]-
CAS No.:906649-01-2
Molecular Formula:C35H47N3O6S
Molecular Weight:637.841
Hs Code.:

Methanesulfonamide,
N-[5-[2-[[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-2H-3,1-benzoxazin-1(4H)-yl
)propyl]amino]-1-hydroxyethyl]-2-(phenylmethoxy)phenyl]-

Synonyms:

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Chemical Property of Methanesulfonamide, N-[5-[2-[[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-2H-3,1-benzoxazin-1(4H)-yl )propyl]amino]-1-hydroxyethyl]-2-(phenylmethoxy)phenyl]-

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Technology Process of Methanesulfonamide, N-[5-[2-[[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-2H-3,1-benzoxazin-1(4H)-yl )propyl]amino]-1-hydroxyethyl]-2-(phenylmethoxy)phenyl]-

There total 2 articles about Methanesulfonamide, N-[5-[2-[[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-2H-3,1-benzoxazin-1(4H)-yl )propyl]amino]-1-hydroxyethyl]-2-(phenylmethoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73883-66-6
N-[2-benzyloxy-5-[2-ethoxy-2-hydroxy-acetyl)-phenyl]-methanesulphonamide

: 906649-01-2
N-(2-benzyloxy-5-{2-[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-4H-benzo[d][1,3]oxazin-1-yl)-propylamino]-1-hydroxy-ethyl}-phenyl)-methanesulphonamide

Guidance literature:: 1-(3-amino-3-methyl-butyl)-4,4-dipropyl-1,4-dihydro-benzo[d][1,3]oxazin-2-one hydrochloride salt; With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.5h;

N-[2-benzyloxy-5-[2-ethoxy-2-hydroxy-acetyl)-phenyl]-methanesulphonamide; In tetrahydrofuran; at 20 ℃; for 2h;

With lithium borohydride; In tetrahydrofuran; at 10 - 20 ℃; for 1h;

Reference yield:

: 73883-66-6
N-[2-benzyloxy-5-[2-ethoxy-2-hydroxy-acetyl)-phenyl]-methanesulphonamide

: 861871-27-4
1-(3-amino-3-methyl-butyl)-4,4-dipropyl-1,4-dihydro-benzo[d][1,3]oxazin-2-one

: 906649-01-2
N-(2-benzyloxy-5-{2-[1,1-dimethyl-3-(2-oxo-4,4-dipropyl-4H-benzo[d][1,3]oxazin-1-yl)-propylamino]-1-hydroxy-ethyl}-phenyl)-methanesulphonamide

Guidance literature:: N-[2-benzyloxy-5-[2-ethoxy-2-hydroxy-acetyl)-phenyl]-methanesulphonamide; 1-(3-amino-3-methyl-butyl)-4,4-dipropyl-1,4-dihydro-benzo[d][1,3]oxazin-2-one; With triethylamine; In tetrahydrofuran; at 20 ℃; for 2.5h;

With lithium borohydride; In tetrahydrofuran; at 10 - 20 ℃; for 1h;