Cyclododecanone, (2,4-dinitrophenyl)hydrazone

Base Information

Chemical Name:Cyclododecanone, (2,4-dinitrophenyl)hydrazone
CAS No.:907-99-3
Molecular Formula:C18H26N4O4
Molecular Weight:362.429
Hs Code.:

Synonyms:

Suppliers and Price of Cyclododecanone, (2,4-dinitrophenyl)hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Cyclododecanone, (2,4-dinitrophenyl)hydrazone

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclododecanone, (2,4-dinitrophenyl)hydrazone

There total 7 articles about Cyclododecanone, (2,4-dinitrophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 830-13-7
cyclododecanone

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 907-99-3
Cyclododecanone 2,4-Dinitrophenylhydrazone

Guidance literature:: DOI:10.1002/hlca.19470300637

Reference yield:

: 73367-80-3
12-bromododecanoic acid

: 907-99-3
Cyclododecanone 2,4-Dinitrophenylhydrazone

Guidance literature:: Multi-step reaction with 7 steps

1: SOCl₂ / 3 h / Heating

2: 85.8 percent / Et₃N / diethyl ether / 0.5 h / Ambient temperature

3: 83.8 percent / NaBH₄, NaH, 2-propanol / dioxane / 1.) 70 deg C, 2.) reflux, 1 h

4: 95.5 percent / m-chloroperbenzoic acid / CH₂Cl₂ / Ambient temperature

5: tert-BuOK / dimethylsulfoxide; tetrahydrofuran / 0.17 h / Ambient temperature

6: Al-Hg / tetrahydrofuran; H₂O / 0.67 h / Heating

7: conc. H₂SO₄ / ethanol / 0.33 h / Heating

With sodium tetrahydroborate; thionyl chloride; aluminium amalgam; sulfuric acid; potassium tert-butylate; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; isopropyl alcohol; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 73674-36-9
2-(2-Methylamino-phenylsulfonyl)-cyclododecanon

: 907-99-3
Cyclododecanone 2,4-Dinitrophenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: Al-Hg / tetrahydrofuran; H₂O / 0.67 h / Heating

2: conc. H₂SO₄ / ethanol / 0.33 h / Heating

With aluminium amalgam; sulfuric acid; In tetrahydrofuran; ethanol; water;