Benzenemethanol, 3-[[3-chloro-5-(1,1-dimethylethyl)-2-hydroxyphenyl]methyl]-5-(1,1-dimeth ylethyl)-2-hydroxy-

Base Information

• Chemical Name: Benzenemethanol, 3-[[3-chloro-5-(1,1-dimethylethyl)-2-hydroxyphenyl]methyl]-5-(1,1-dimeth ylethyl)-2-hydroxy-
• CAS No.: 908-17-8
• Molecular Formula: C₂₂H₂₉ClO₃
• Molecular Weight: 376.923
• Mol file: 908-17-8.mol

Synonyms:

Chemical Property of Benzenemethanol, 3-[[3-chloro-5-(1,1-dimethylethyl)-2-hydroxyphenyl]methyl]-5-(1,1-dimeth ylethyl)-2-hydroxy-

Chemical Property:

• Melting Point: 140 °C
• Boiling Point: 464.3±40.0 °C(Predicted)
• PSA: 60.69000
• Density: 1.160±0.06 g/cm3(Predicted)
• LogP: 5.42930

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, 3-[[3-chloro-5-(1,1-dimethylethyl)-2-hydroxyphenyl]methyl]-5-(1,1-dimeth ylethyl)-2-hydroxy-

There total 2 articles about Benzenemethanol, 3-[[3-chloro-5-(1,1-dimethylethyl)-2-hydroxyphenyl]methyl]-5-(1,1-dimeth ylethyl)-2-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-tert-butylphenol (98-54-4) → 3-Chlor-2,2'-dihydroxy-3'-hydroxymethyl-5,5'-di-tert-butyl-diphenylmethan (908-17-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / ethanol

2: aq. NaOH / methanol

With hydrogenchloride; sodium hydroxide; In methanol; ethanol;

DOI:10.1007/BF00901717

Reference yield:

5-Chlor-4-hydroxy-3-hydroxymethyl-1-tert.-butyl-benzol (16396-75-1) → 3-Chlor-2,2'-dihydroxy-3'-hydroxymethyl-5,5'-di-tert-butyl-diphenylmethan (908-17-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / ethanol

2: aq. NaOH / methanol

With hydrogenchloride; sodium hydroxide; In methanol; ethanol;

DOI:10.1007/BF00901717

Reference yield:

3-Chlor-2,2'-dihydroxy-3'-hydroxymethyl-5,5'-di-tert-butyl-diphenylmethan (908-17-8) → 3-<3-<3-(5-tert-butylsalicyl)-5-tert-butylsalicyl>-5-tert-butylsalicyl>-5-tert-butyl-2-hydroxybenzyl alcohol (68803-63-4)

Guidance literature:

Multi-step reaction with 5 steps

1: aq. HCl

2: aq. NaOH / methanol

3: aq. HCl

4: aq. NaOH / methanol

5: H₂, aq. KOH / Raney-Ni / dioxane; methanol

With hydrogenchloride; potassium hydroxide; sodium hydroxide; hydrogen; nickel; In 1,4-dioxane; methanol;

DOI:10.1007/BF00907297

upstream raw materials:

para-tert-butylphenol

5-Chlor-4-hydroxy-3-hydroxymethyl-1-tert.-butyl-benzol

Downstream raw materials:

4-tert.-Butyl-2,6-bis-(3-chlor-2-hydroxy-5-tert.-butyl-benzyl)-phenol

C₇₆H₉₆Cl₂O₇

2,2'-Dihydroxy-5,5'-di-tert-butyl-3,3'-bis-(3-chlor-2-hydroxy-5-tert-butyl-benzyl)-diphenylmethan

C₁₂₀H₁₅₂Cl₂O₁₁