Morpholine, 4-[3-[3-[2,4-bis(methoxymethoxy)-5-(1-methylethyl)phenyl]-5-(methylsulf onyl)-4H-1,2,4-triazol-4-yl]propyl]-

Base Information

Chemical Name:Morpholine, 4-[3-[3-[2,4-bis(methoxymethoxy)-5-(1-methylethyl)phenyl]-5-(methylsulf onyl)-4H-1,2,4-triazol-4-yl]propyl]-
CAS No.:909872-35-1
Molecular Formula:C23H36N4O7S
Molecular Weight:512.627
Hs Code.:

Synonyms:

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Chemical Property of Morpholine, 4-[3-[3-[2,4-bis(methoxymethoxy)-5-(1-methylethyl)phenyl]-5-(methylsulf onyl)-4H-1,2,4-triazol-4-yl]propyl]-

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Morpholine, 4-[3-[3-[2,4-bis(methoxymethoxy)-5-(1-methylethyl)phenyl]-5-(methylsulf onyl)-4H-1,2,4-triazol-4-yl]propyl]-

There total 10 articles about Morpholine, 4-[3-[3-[2,4-bis(methoxymethoxy)-5-(1-methylethyl)phenyl]-5-(methylsulf onyl)-4H-1,2,4-triazol-4-yl]propyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.1%

: 909872-34-0
C₂₃H₃₆N₄O₅S

: 909872-35-1
C₂₃H₃₆N₄O₇S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 20h;

Reference yield:

: 123-00-2
4-(3-Aminopropyl)morpholine

: 909872-35-1
C₂₃H₃₆N₄O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / dichloromethane / 2 h

2: ethanol / 2 h / Heating / reflux

3: potassium hydroxide / ethanol; water / 1.5 h / Heating / reflux

4: potassium carbonate / ethanol / 1 h / Heating / reflux

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h

With pyridine; potassium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; water;

Reference yield:

: 909870-97-9
4-bromo-6-isopropyl-benzene-1,3-diol

: 909872-35-1
C₂₃H₃₆N₄O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18.5 h / 20 - 50 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 - -40 °C

2.2: -40 - 20 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine / N,N-dimethyl-formamide / 20 h

4.1: ethanol / 2 h / Heating / reflux

5.1: potassium hydroxide / ethanol; water / 1.5 h / Heating / reflux

6.1: potassium carbonate / ethanol / 1 h / Heating / reflux

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h

With potassium hydroxide; n-butyllithium; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; hydrazine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;