2-Propanol, 1-amino-3-[2,6-dimethyl-4-[5-(4,5,6,7-tetrahydro-3,5,5-trimethylbenzo[c] thien-1-yl)-1,2,4-oxadiazol-3-yl]phenoxy]-

Base Information

Chemical Name:2-Propanol, 1-amino-3-[2,6-dimethyl-4-[5-(4,5,6,7-tetrahydro-3,5,5-trimethylbenzo[c] thien-1-yl)-1,2,4-oxadiazol-3-yl]phenoxy]-
CAS No.:910639-69-9
Molecular Formula:C₂₄H₃₁N₃O₃S
Molecular Weight:441.594
Hs Code.:

Synonyms:

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Chemical Property of 2-Propanol, 1-amino-3-[2,6-dimethyl-4-[5-(4,5,6,7-tetrahydro-3,5,5-trimethylbenzo[c] thien-1-yl)-1,2,4-oxadiazol-3-yl]phenoxy]-

Chemical Property:

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Technology Process of 2-Propanol, 1-amino-3-[2,6-dimethyl-4-[5-(4,5,6,7-tetrahydro-3,5,5-trimethylbenzo[c] thien-1-yl)-1,2,4-oxadiazol-3-yl]phenoxy]-

There total 13 articles about 2-Propanol, 1-amino-3-[2,6-dimethyl-4-[5-(4,5,6,7-tetrahydro-3,5,5-trimethylbenzo[c] thien-1-yl)-1,2,4-oxadiazol-3-yl]phenoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₈N₂O₃S

: 910639-69-9
C₂₄H₃₁N₃O₃S

Guidance literature:: With ammonia; In methanol; at 65 ℃; for 18h; Sealed tube;
DOI:10.1021/jm401456d

Reference yield:

: 162854-15-1
N,4-dihydroxy-3,5-dimethylbenzimidamide

: 910639-69-9
C₂₄H₃₁N₃O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 18 h / 20 °C

2.1: sodium hydroxide / isopropyl alcohol; water / 20 h / 20 °C

3.1: ammonia / methanol / 18 h / 65 °C / Sealed tube

With ammonia; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm401456d

Reference yield:

: 1073-13-8
4,4-dimethylcyclohexenone

: 910639-69-9
C₂₄H₃₁N₃O₃S

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrogen; palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C / 750.08 Torr

2.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.5 h / 20 °C / Cooling with ice

2.2: 0.83 h / 15 - 20 °C

3.1: oxalyl dichloride / chloroform / 1 h / 20 - 25 °C

4.1: sodium; ethanol / tetrahydrofuran / 1 h / 20 °C

5.1: sodium; ethanol / 0.25 h / 50 - 75 °C

6.1: water; lithium hydroxide / ethanol / 70 °C

7.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.25 h / -78 °C

7.2: 0.5 h / -78 °C

8.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 20 °C

8.2: 18 h / 20 °C

9.1: sodium hydroxide / isopropyl alcohol; water / 20 h / 20 °C

10.1: ammonia / methanol / 18 h / 65 °C / Sealed tube

With oxalyl dichloride; ethanol; palladium 10% on activated carbon; potassium tert-butylate; ammonia; water; hydrogen; tert.-butyl lithium; sodium; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; chloroform; water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; tert-butyl alcohol; pentane;
DOI:10.1021/jm401456d