Cyclohexanemethanamine, 5-amino-1,3,3-trimethyl-, (1S,5R)-

Base Information

Chemical Name:Cyclohexanemethanamine, 5-amino-1,3,3-trimethyl-, (1S,5R)-
CAS No.:911028-53-0
Molecular Formula:C10H22N2
Molecular Weight:170.298
Hs Code.:

Synonyms:(1R,3S)-3-(aminomethyl)-3,5,5-trimethyl-cyclohexylamine;(1R,3S)-3-aminomethyl-3,5,5-trimethylcyclohexylamine;(1R,3S)-3-Aminomethyl-3,5,5-trimethyl-cyclohexylamine;(1R,3S)-3-(aminomethyl)-3,5,5-trimethylcyclohexanamine;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanemethanamine, 5-amino-1,3,3-trimethyl-, (1S,5R)-

Chemical Property:

PSA：52.04000
LogP:2.88940

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanemethanamine, 5-amino-1,3,3-trimethyl-, (1S,5R)-

There total 3 articles about Cyclohexanemethanamine, 5-amino-1,3,3-trimethyl-, (1S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 918963-24-3
benzyl N-{(1R,3S)-3-[(benzyloxycarbonylamino)methyl]-3,5,5-trimethylcyclohexyl}carbamate

: 911028-53-0
(1R,3S)-3-(aminomethyl)-3,5,5-trimethyl-cyclohexylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 12h; under 760 Torr;
DOI:10.1021/jo0613737

Reference yield:

: benzyl cis-N-{3-[(benzyloxycarbonylamino)methyl]-3,5,5-trimethylcyclohexyl}carbamate

: 911028-53-0
(1R,3S)-3-(aminomethyl)-3,5,5-trimethyl-cyclohexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: Diacel Chiralpak AD column / hexane; propan-2-ol

2: 100 percent / hydrogen / Pd/C / methanol / 12 h / 20 °C / 760 Torr

With Diacel Chiralpak AD column; hydrogen; palladium on activated charcoal; In methanol; hexane; isopropyl alcohol;
DOI:10.1021/jo0613737

Reference yield:

: 918963-28-7
(2R,3R)-2,3-bis(benzyloxy)butanedioic acid (1S,5R)-(5-amino-1,3,3-trimethylcyclohexyl)methaneamine salt (1:1)

: 911028-53-0
(1R,3S)-3-(aminomethyl)-3,5,5-trimethyl-cyclohexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / H₂O

2: 100 percent / hydrogen / Pd/C / methanol / 12 h / 20 °C / 760 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; water;
DOI:10.1021/jo0613737