5-Methoxy-3-phenyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine

Base Information

Chemical Name:5-Methoxy-3-phenyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine
CAS No.:91322-02-0
Molecular Formula:C11H9N5O
Molecular Weight:227.225
Hs Code.:
DSSTox Substance ID:DTXSID50554144
Wikidata:Q82435003

Synonyms:91322-02-0;5-Methoxy-3-phenyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine;DTXSID50554144

Suppliers and Price of 5-Methoxy-3-phenyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 5-Methoxy-3-phenyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:227.08070993
Heavy Atom Count:17
Complexity:258

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=NC=C2C(=N1)N(N=N2)C3=CC=CC=C3

Technology Process of 5-Methoxy-3-phenyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine

There total 9 articles about 5-Methoxy-3-phenyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 139300-73-5
7-iodo-5-methoxy-3-phenyl-3H-1,2,3-triazolo<4,5-d>pyrimidine

: 91322-02-0
5-Methoxy-3-phenyl-3H-1,2,3-triazolo<4,5-d>pyrimidine

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -100 ℃; for 0.00833333h;
DOI:10.1248/cpb.39.2793

Reference yield:

: 91322-01-9
5-chloro-3-phenyl-3H-1,2,3-triazolo<4,5-d>pyrimidine

: 91322-02-0
5-Methoxy-3-phenyl-3H-1,2,3-triazolo<4,5-d>pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / dimethylformamide; H₂O / 1 h / 60 °C

2: 65 percent / KMnO₄ / H₂O; acetic acid / 2 h / Ambient temperature

3: 97 percent / methanol / 1 h / Ambient temperature

With potassium permanganate; In methanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.1731

Reference yield:

: 124799-17-3
5-(methylthio)-3-phenyl-3H-1,2,3-triazolo<4,5-d>pyrimidine

: 91322-02-0
5-Methoxy-3-phenyl-3H-1,2,3-triazolo<4,5-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / KMnO₄ / H₂O; acetic acid / 2 h / Ambient temperature

2: 97 percent / methanol / 1 h / Ambient temperature

With potassium permanganate; In methanol; water; acetic acid;
DOI:10.1248/cpb.37.1731