N-(2-Succinyl) Phenylephrine (Mixture of Diastereomers)

Base Information

• Chemical Name: N-(2-Succinyl) Phenylephrine (Mixture of Diastereomers)
• CAS No.: 915278-80-7
• Molecular Formula: C₁₃H₁₇NO₆
• Molecular Weight: 283.281
• Mol file: 915278-80-7.mol

Synonyms:N-(2-Succinyl) Phenylephrine;

Chemical Property of N-(2-Succinyl) Phenylephrine (Mixture of Diastereomers)

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 120-125°C
• Boiling Point: 520.8±50.0 °C (760 mmHg)
• PKA: 2.13±0.23(Predicted)
• PSA: 118.30000
• Density: 1.428±0.06 g/cm3 (20 °C, 760 mmHg)
• LogP: 0.28530
• Storage Temp.: Refrigerator
• Solubility.: Methanol, Water

Purity/Quality:

97% ^*data from raw suppliers

N-(2-Succinyl)Phenylephrine(MixtureofDiastereomers) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: The major degradation product identified in The major degradation product identified in Acetaminophen, Phenylephrine hydrochloride, and Chlorpheniramine maleate.

Technology Process of N-(2-Succinyl) Phenylephrine (Mixture of Diastereomers)

There total 2 articles about N-(2-Succinyl) Phenylephrine (Mixture of Diastereomers) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibenzyl N-{(2R)-2-[3-(benzyloxy)phenyl]-2-hydroxyethyl}-N-methylaspartate → N-{(2R)-2-hydroxy-2-(3-hydroxyphenyl)ethyl}-N-methylaspartic acid (915278-80-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/ac0611263

Reference yield:

(1R)-1-[3-(benzyloxy)phenyl]-2-(methylamino)ethanol → N-{(2R)-2-hydroxy-2-(3-hydroxyphenyl)ethyl}-N-methylaspartic acid (915278-80-7)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/ac0611263

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