Technology Process of Benzene, (1-cyclohexyl-4-methyl-3-penten-1-yl)-
There total 8 articles about Benzene, (1-cyclohexyl-4-methyl-3-penten-1-yl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
isopropyltriphenylphosphonium iodide;
With
n-butyllithium;
In
tetrahydrofuran;
3-Cyclohexyl-3-phenylpropanal;
In
tetrahydrofuran;
DOI:10.1016/j.tet.2006.07.102
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 95 percent / LiAlH4 / diethyl ether / 8 h / 20 °C
2.1: 70 percent / BF3*Et2O; triethylsilane / CH2Cl2 / 0 °C
3.1: 75 percent / PCC / CH2Cl2
4.1: n-BuLi / tetrahydrofuran
4.2: 59 percent / tetrahydrofuran
With
triethylsilane; lithium aluminium tetrahydride; n-butyllithium; boron trifluoride diethyl etherate; pyridinium chlorochromate;
In
tetrahydrofuran; diethyl ether; dichloromethane;
4.2: Wittig coupling;
DOI:10.1016/j.tet.2006.07.102
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 75 percent / activated Zn / benzene; diethyl ether / 24 h / Heating
2.1: 95 percent / LiAlH4 / diethyl ether / 8 h / 20 °C
3.1: 70 percent / BF3*Et2O; triethylsilane / CH2Cl2 / 0 °C
4.1: 75 percent / PCC / CH2Cl2
5.1: n-BuLi / tetrahydrofuran
5.2: 59 percent / tetrahydrofuran
With
triethylsilane; lithium aluminium tetrahydride; n-butyllithium; boron trifluoride diethyl etherate; pyridinium chlorochromate; zinc;
In
tetrahydrofuran; diethyl ether; dichloromethane; benzene;
1.1: Reformatsky coupling / 5.2: Wittig coupling;
DOI:10.1016/j.tet.2006.07.102