2H-Pyran-2-one,5,6-dihydro-3-[(3E)-4-methyl-6-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-hexen-1-yl]-6-[(3S)-tetrahydro-5-oxo-3-furanyl]-,(6R)-

Base Information

Chemical Name:2H-Pyran-2-one,5,6-dihydro-3-[(3E)-4-methyl-6-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-hexen-1-yl]-6-[(3S)-tetrahydro-5-oxo-3-furanyl]-,(6R)-
CAS No.:141344-10-7
Molecular Formula:C₂₅H₃₆O₄
Molecular Weight:400.558
Hs Code.:

Synonyms:2H-Pyran-2-one,5,6-dihydro-3-[(3E)-4-methyl-6-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-hexenyl]-6-[(3S)-tetrahydro-5-oxo-3-furanyl]-,(6R)- (9CI); 2H-Pyran-2-one,5,6-dihydro-3-[4-methyl-6-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-hexenyl]-6-(tetrahydro-5-oxo-3-furanyl)-,[R-[R*,S*-(E)]]-; (+)-Luffariolide E; Luffariolide E

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Chemical Property of 2H-Pyran-2-one,5,6-dihydro-3-[(3E)-4-methyl-6-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-hexen-1-yl]-6-[(3S)-tetrahydro-5-oxo-3-furanyl]-,(6R)-

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MSDS Files:: SDS file from LookChem

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Technology Process of 2H-Pyran-2-one,5,6-dihydro-3-[(3E)-4-methyl-6-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-hexen-1-yl]-6-[(3S)-tetrahydro-5-oxo-3-furanyl]-,(6R)-

There total 4 articles about 2H-Pyran-2-one,5,6-dihydro-3-[(3E)-4-methyl-6-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-hexen-1-yl]-6-[(3S)-tetrahydro-5-oxo-3-furanyl]-,(6R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141321-14-4
2,3-dihydroluffariolide B

: 141344-10-7
luffariolide E

Guidance literature:: With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo00038a051

Reference yield:

: 141321-13-3
luffariolide D

: 141344-10-7
luffariolide E

Guidance literature:: With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jo00038a051

Reference yield:

: 121402-07-1
luffariolide B

: 141344-10-7
luffariolide E

Guidance literature:: Multi-step reaction with 2 steps

1: 1.0 mg / NaBH₄ / ethanol / 2 h / Ambient temperature

2: 1.2 mg / PCC, molecular sieves 4 Angstroem / CH₂Cl₂ / 2 h / Ambient temperature

With sodium tetrahydroborate; 4 A molecular sieve; pyridinium chlorochromate; In ethanol; dichloromethane;
DOI:10.1021/jo00038a051