Ethanone, 1-(2-amino-5-methoxyphenyl)-2-phenyl-

Base Information

Chemical Name:Ethanone, 1-(2-amino-5-methoxyphenyl)-2-phenyl-
CAS No.:917610-37-8
Molecular Formula:C15H15NO2
Molecular Weight:241.29
Hs Code.:
DSSTox Substance ID:DTXSID90475420
Wikidata:Q82305944

Synonyms:917610-37-8;Ethanone, 1-(2-amino-5-methoxyphenyl)-2-phenyl-;DTXSID90475420

Suppliers and Price of Ethanone, 1-(2-amino-5-methoxyphenyl)-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-(2-amino-5-methoxyphenyl)-2-phenyl-

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:241.110278721
Heavy Atom Count:18
Complexity:274

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)N)C(=O)CC2=CC=CC=C2

Technology Process of Ethanone, 1-(2-amino-5-methoxyphenyl)-2-phenyl-

There total 1 articles about Ethanone, 1-(2-amino-5-methoxyphenyl)-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 50916-21-7
N-(4-methoxyphenyl)-2-phenylacetamide

: 917610-37-8
1-(2-amino-5-methoxy-phenyl)-2-phenyl-ethanone

Guidance literature:: In acetonitrile; at 20 ℃; for 24h; Irradiation;
DOI:10.1021/jo0614442

Reference yield: 80.0%

: 917610-37-8
1-(2-amino-5-methoxy-phenyl)-2-phenyl-ethanone

: 15761-38-3
L-N-Boc-Ala

: [1-(4-methoxy-2-phenylacetyl-phenylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/jo0614442

Reference yield:

: 917610-37-8
1-(2-amino-5-methoxy-phenyl)-2-phenyl-ethanone

: 5-benzyl-7-methoxy-3-methyl-1,3-dihydro-benzo[e][1,4]diazepin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DCC; DMAP / dimethylformamide / 12 h / 20 °C

2: 72 percent / TFA; Et₃SiH / CH₂Cl₂ / 4 h / 20 °C

With triethylsilane; dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0614442