1,4-Dioxaspiro[4.5]dec-6-en-8-ol, 8-[(1E,3E)-3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-5-hydroxy-1,3 -pentadien-1-yl]-2,3,7,9,9-pentamethyl-, (2S,3S,8S)-

Base Information

Chemical Name:1,4-Dioxaspiro[4.5]dec-6-en-8-ol, 8-[(1E,3E)-3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-5-hydroxy-1,3 -pentadien-1-yl]-2,3,7,9,9-pentamethyl-, (2S,3S,8S)-
CAS No.:917752-75-1
Molecular Formula:C35H48O5Si
Molecular Weight:576.849
Hs Code.:

1,4-Dioxaspiro[4.5]dec-6-en-8-ol,
8-[(1E,3E)-3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-5-hydroxy-1,3
-pentadien-1-yl]-2,3,7,9,9-pentamethyl-, (2S,3S,8S)-

Synonyms:

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Chemical Property of 1,4-Dioxaspiro[4.5]dec-6-en-8-ol, 8-[(1E,3E)-3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-5-hydroxy-1,3 -pentadien-1-yl]-2,3,7,9,9-pentamethyl-, (2S,3S,8S)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,4-Dioxaspiro[4.5]dec-6-en-8-ol, 8-[(1E,3E)-3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-5-hydroxy-1,3 -pentadien-1-yl]-2,3,7,9,9-pentamethyl-, (2S,3S,8S)-

There total 1 articles about 1,4-Dioxaspiro[4.5]dec-6-en-8-ol, 8-[(1E,3E)-3-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-5-hydroxy-1,3 -pentadien-1-yl]-2,3,7,9,9-pentamethyl-, (2S,3S,8S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 917752-74-0
(2S,3S,8S)-8-(5-hydroxy-3-[tert-butyldiphenylsiloxymethyl]pent-3-en-1-ynyl)-2,3,7,9,9-pentamethyl-1,4-dioxaspiro[4.5]dec-6-en-8-ol

: 917752-75-1
(2S,3S,8S)-8-(5-hydroxy-3-[tert-butyldiphenylsiloxymethyl]-1,3-pentadienyl)-2,3,7,9,9-pentamethyl-1,4-dioxaspiro[4.5]dec-6-en-8-ol

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 0.5h;
DOI:10.1039/b611880a

Reference yield: 86.0%

: 917752-75-1
(2S,3S,8S)-8-(5-hydroxy-3-[tert-butyldiphenylsiloxymethyl]-1,3-pentadienyl)-2,3,7,9,9-pentamethyl-1,4-dioxaspiro[4.5]dec-6-en-8-ol

: 917752-76-2
(2S,3S,8S)-8-(3-[tert-butyldiphenylsiloxymethyl]penta-2,4-dienal)-2,3,7,9,9-pentamethyl-1,4-dioxaspiro[4.5]dec-6-en-8-ol

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; for 0.25h;
DOI:10.1039/b611880a