4-(2-(2-Ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)morpholine

Base Information

Chemical Name:4-(2-(2-Ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)morpholine
CAS No.:130688-25-4
Molecular Formula:C₂₀H₃₁NO₂
Molecular Weight:317.472
Hs Code.:
DSSTox Substance ID:DTXSID40926856

Synonyms:BRN 4355638;4-(2-(2-Ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)morpholine;Morpholine, 4-(2-(2-ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)-;130688-25-4;DTXSID40926856;4-[2-(2-ethyl-2-methyl-4-phenyloxan-4-yl)ethyl]morpholine;LS-93023

Suppliers and Price of 4-(2-(2-Ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)morpholine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-(2-(2-Ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)morpholine

Chemical Property:

Vapor Pressure:3.34E-07mmHg at 25°C
Boiling Point:418.2°Cat760mmHg
Flash Point:123.9°C
Density:0.997g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:317.235479232
Heavy Atom Count:23
Complexity:363

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1(CC(CCO1)(CCN2CCOCC2)C3=CC=CC=C3)C

Technology Process of 4-(2-(2-Ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)morpholine

There total 3 articles about 4-(2-(2-Ethyltetrahydro-2-methyl-4-phenyl-2H-pyran-4-yl)ethyl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 130688-19-6
2-(2-Ethyl-2-methyl-4-phenyl-tetrahydro-pyran-4-yl)-1-morpholin-4-yl-ethanone

: 130688-25-4
2-methyl-2-ethyl-4-phenyl-4-β-N-morphylylethyltetrahydropyran

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; for 20h; Heating;
DOI:10.1007/BF00766251

Reference yield:

: 109878-52-6
(2-Ethyl-2-methyl-4-phenyl-tetrahydro-pyran-4-yl)-acetic acid

: 130688-25-4
2-methyl-2-ethyl-4-phenyl-4-β-N-morphylylethyltetrahydropyran

Guidance literature:: Multi-step reaction with 3 steps

1: formamide, SOCl₂ / benzene / 1 h / 60 °C

2: diethyl ether / 24 h

3: 65 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 20 h / Heating

With lithium aluminium tetrahydride; thionyl chloride; formamide; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1007/BF00766251

Reference yield:

: 130688-10-7
2-methyl-2-ethyl-4-benzyltetrahydropyran-4-ylcarbonyl chloride

: 130688-25-4
2-methyl-2-ethyl-4-phenyl-4-β-N-morphylylethyltetrahydropyran

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 24 h

2: 65 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 20 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1007/BF00766251