2-Oxazolidinone, 3-[(2R,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-7-[[(1,1-dimethylethyl) diphenylsilyl]oxy]-2-methyl-1-oxoheptyl]-4-(phenylmethyl)-, (4R)-

Base Information

Chemical Name:2-Oxazolidinone, 3-[(2R,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-7-[[(1,1-dimethylethyl) diphenylsilyl]oxy]-2-methyl-1-oxoheptyl]-4-(phenylmethyl)-, (4R)-
CAS No.:917767-28-3
Molecular Formula:C40H57NO5Si2
Molecular Weight:688.067
Hs Code.:

2-Oxazolidinone,
3-[(2R,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-7-[[(1,1-dimethylethyl)
diphenylsilyl]oxy]-2-methyl-1-oxoheptyl]-4-(phenylmethyl)-, (4R)-

Synonyms:

Suppliers and Price of 2-Oxazolidinone, 3-[(2R,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-7-[[(1,1-dimethylethyl) diphenylsilyl]oxy]-2-methyl-1-oxoheptyl]-4-(phenylmethyl)-, (4R)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Oxazolidinone, 3-[(2R,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-7-[[(1,1-dimethylethyl) diphenylsilyl]oxy]-2-methyl-1-oxoheptyl]-4-(phenylmethyl)-, (4R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Oxazolidinone, 3-[(2R,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-7-[[(1,1-dimethylethyl) diphenylsilyl]oxy]-2-methyl-1-oxoheptyl]-4-(phenylmethyl)-, (4R)-

There total 3 articles about 2-Oxazolidinone, 3-[(2R,3S)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-7-[[(1,1-dimethylethyl) diphenylsilyl]oxy]-2-methyl-1-oxoheptyl]-4-(phenylmethyl)-, (4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 917767-37-4
(R)-4-benzyl-3-((2R,3S)-7-(tert-butyldiphenylsilyloxy)-3-hydroxy-2-methylheptanoyl)oxazolidin-2-one

: 69739-34-0
t-butyldimethylsiyl triflate

: 917767-28-3
(R)-4-benzyl-3-((2R,3S)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-2-methylheptanoyl)oxazolidin-2-one

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 8h;
DOI:10.1039/b609408b

Reference yield:

: 101711-78-8,131685-53-5
(3R)-3-propionyl-4-benzyloxazolidin-2-one

: 917767-28-3
(R)-4-benzyl-3-((2R,3S)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-2-methylheptanoyl)oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine; Bu₂BOTf / CH₂Cl₂ / -78 - 0 °C

2: 98 percent / ethyl-N,N-diisopropylamine / CH₂Cl₂ / 8 h / 0 °C

With di-n-butylboryl trifluoromethanesulfonate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/b609408b

Reference yield:

: 131216-47-2
5-(tert-butyldiphenylsilyloxy)pentanal

: 917767-28-3
(R)-4-benzyl-3-((2R,3S)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-2-methylheptanoyl)oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine; Bu₂BOTf / CH₂Cl₂ / -78 - 0 °C

2: 98 percent / ethyl-N,N-diisopropylamine / CH₂Cl₂ / 8 h / 0 °C

With di-n-butylboryl trifluoromethanesulfonate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/b609408b