2',3'-epoxypropylglucopyranoside

Base Information

Chemical Name:2',3'-epoxypropylglucopyranoside
CAS No.:33275-57-9
Molecular Formula:C₉H₁₆O₇
Molecular Weight:236.222
Hs Code.:
Mol file:33275-57-9.mol

Synonyms:Glucopyranoside,2,3-epoxypropyl, b-D-(8CI); (R,S)-2',3'-Epoxypropyl-b-D-glucopyranoside

Suppliers and Price of 2',3'-epoxypropylglucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2',3'-epoxypropylglucopyranoside

Chemical Property:

Vapor Pressure:2.2E-11mmHg at 25°C
Boiling Point:483.7°Cat760mmHg
Flash Point:246.3°C
PSA：111.91000
Density:1.54g/cm³
LogP:-2.79830

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2',3'-epoxypropylglucopyranoside

There total 4 articles about 2',3'-epoxypropylglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33275-56-8
2,3-epoxypropyl tetra-O-acetyl-β-D-glucopyranoside

: 33275-57-9
2,3-epoxypropyl β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; for 0.5h;
DOI:10.1071/CH9900665

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 33275-57-9
2,3-epoxypropyl β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) mercury(II) oxide, mercury(II) bromide, calcium sulfate / 1.) dichloromethane, RT, 30 min

2: 64 percent / m-chloroperbenzoic acid, 2,6-di-t-butyl-4-methylphenol / CH₂Cl₂ / 4 h / Heating

3: 79 mg / sodium methoxide / methanol / 0.5 h

With calcium sulfate; 2,6-di-tert-butyl-4-methyl-phenol; sodium methylate; 3-chloro-benzenecarboperoxoic acid; mercury dibromide; mercury(II) oxide; In methanol; dichloromethane;
DOI:10.1071/CH9900665

Reference yield:

: 10343-15-4,39698-55-0,54400-76-9,78730-32-2,119111-31-8,119111-32-9
Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-allyloxy-tetrahydro-pyran-4-yl ester

: 33275-57-9
2,3-epoxypropyl β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / m-chloroperbenzoic acid, 2,6-di-t-butyl-4-methylphenol / CH₂Cl₂ / 4 h / Heating

2: 79 mg / sodium methoxide / methanol / 0.5 h

With 2,6-di-tert-butyl-4-methyl-phenol; sodium methylate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1071/CH9900665