2(1H)-Pyridinone, 3-bromo-4-(4-chlorophenyl)-6-methyl-

Base Information

Chemical Name:2(1H)-Pyridinone, 3-bromo-4-(4-chlorophenyl)-6-methyl-
CAS No.:917969-65-4
Molecular Formula:C12H9BrClNO
Molecular Weight:298.567
Hs Code.:

Synonyms:3-bromo-4-(4-chlorophenyl)-6-methylpyridin-2(1H)-one;2(1H)-Pyridinone,3-bromo-4-(4-chlorophenyl)-6-methyl;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2(1H)-Pyridinone, 3-bromo-4-(4-chlorophenyl)-6-methyl-

Chemical Property:

PSA：32.86000
LogP:3.76620

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2(1H)-Pyridinone, 3-bromo-4-(4-chlorophenyl)-6-methyl-

There total 2 articles about 2(1H)-Pyridinone, 3-bromo-4-(4-chlorophenyl)-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 24452-07-1
4-(4-chloro-phenyl)-6-methyl-1H-pyridin-2-one

: 917969-65-4
3-bromo-4-(4-chlorophenyl)-6-methylpyridin-2(1H)-one

Guidance literature:: With N-Bromosuccinimide; In methanol; at 20 - 40 ℃; for 1.66667h;

Reference yield:

: 30626-03-0
(3E)-4-(4-chlorophenyl)-3-buten-2-one

: 917969-65-4
3-bromo-4-(4-chlorophenyl)-6-methylpyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / ethanol / 4.25 h / 20 °C / Heating / reflux

2: N-Bromosuccinimide / methanol / 1.67 h / 20 - 40 °C

With N-Bromosuccinimide; ammonium acetate; In methanol; ethanol;

Reference yield: 60.0%

: 917969-65-4
3-bromo-4-(4-chlorophenyl)-6-methylpyridin-2(1H)-one

: 917969-66-5
3-bromo-2-chloro-4-(4-chlorophenyl)-6-methylpyridine

Guidance literature:: 3-bromo-4-(4-chlorophenyl)-6-methylpyridin-2(1H)-one; With trichlorophosphate; N,N-dimethyl-formamide; at 100 ℃; for 7h;

With water; sodium hydrogencarbonate; pH=7 - 8;